1-甲氧基-4-苯氧基苯合成路线 (共 73 条)
反应条件
1: 4-methoxy-phenol With potassium tert-butylate in tetrahydrofuran
T=0°C; 0.25 h;
2: Diphenyliodonium triflate in tetrahydrofuran
T=40°C; 1.83333 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
potassium tert-butylate in dimethyl sulfoxide
T=120°C; Ullmann type coupling; 2 h; Inert atmosphere;
参考文献
Yang, Shuliang; Wu, Cunqi; Ruan, Mingbo; Yang, Yanqin; Zhao, Yongxia; Niu, Jiajia; Yang, Wei; Xu, Jingwei
Tetrahedron Letters, 2012 , vol. 53, # 33 p. 4288 - 4292
反应条件
potassium phosphate in tetrahydrofuran
T=115°C; 18 h;
参考文献
Ghosh, Rajshekhar; Samuelson, Ashoka G.
New Journal of Chemistry, 2004 , vol. 28, # 11 p. 1390 - 1393
反应条件
copper(l) iodide in various solvent(s)
T=130°C; 12 h;
参考文献
Ito, Hajime; Sensui, Hiro-Omi; Arimoto, Kikuo; Miura, Katsukiyo; Hosomi, Akira
Chemistry Letters, 1997 , # 7 p. 639 - 640
反应条件
copper(l) iodide; caesium carbonate in N,N-dimethyl-formamide
T=100°C; 8 h;
参考文献
Cui, Sun-Liang; Jiang, Zhi-Yong; Wang, Yan-Guang
Synlett, 2004 , # 10 p. 1829 - 1831
反应条件
potassium carbonate in acetonitrile
T=50°C; 30 h;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
potassium carbonate in acetonitrile
T=50°C; 24 h;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
potassium hydroxide in dimethyl sulfoxide
T=20°C; 4 h;
参考文献
Elhalem, Eleonora; Bailey, Brian N.; Docampo, Roberto; Ujvary, Istvan; Szajnman, Sergio H.; Rodriguez, Juan B.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 18 p. 3984 - 3999
反应条件
copper diacetate; triethylamine in dichloromethane
T=50°C; 3 h; Sealed tube; Reagent/catalystTime;
参考文献
Crifar, Cynthia; Petiot, Pauline; Ahmad, Tabinda; Gagnon, Alexandre
Chemistry - A European Journal, 2014 , vol. 20, # 10 p. 2755 - 2760
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 20 °C
2.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 °C
2.2: 1.83 h / 40 °C
View Scheme
参考文献
Jalalian, Nazli; Ishikawa, Eloisa E.; Silva, Luiz F.; Olofsson, Berit
Organic Letters, 2011 , vol. 13, # 6 p. 1552 - 1555