双(4-甲氧基二苯基)醚合成路线 （共 17 条）
反应条件
copper(I) oxide; caesium carbonate; 1H-imidazole-4-carboxylic acid in acetonitrile T=80°C; 24 h;
参考文献
Cheng, An-Yi; Hsieh, Jen-Chieh
Tetrahedron Letters, 2012 , vol. 53, # 1 p. 71 - 75
反应条件
ethyl dimethylaminomethylphosphonate hydrochloride; copper(l) iodide; potassium carbonate in toluene T=110°C; Ullmann reaction; 30 h;
参考文献
Jin, Ying; Liu, Jinyong; Yin, Yingwu; Fu, Hua; Jiang, Yuyang; Zhao, Yufen
Synlett, 2006 , # 10 p. 1564 - 1568
反应条件
1: 4-methoxy-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: bis(4-methoxyphenyl)iodonium trifluoromethanesulfonate in tetrahydrofuran T=40°C; 0.833333 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
copper diacetate; water; triethylamine in dichloromethane; acetonitrile T=25°C; 6 h;
参考文献
Sagar; Tale; Adude
Tetrahedron Letters, 2003 , vol. 44, # 37 p. 7061 - 7063
反应条件
potassium phosphate; copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; water in ethanol T=130°C; 30 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Tlili, Anis; Monnier, Florian; Taillefer, Marc
Chemistry - A European Journal, 2010 , vol. 16, # 41 p. 12299 - 12302
反应条件
1.1: iodine; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.25 h / 40 °C 1.2: 1 h / 20 °C 2.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 °C 2.2: 0.83 h / 40 °C View Scheme
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
potassium carbonate in acetonitrile T=50°C; 27 h;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
copper diacetate; 4 A molecular sieve; triethylamine in dichloromethane T=20°C;
参考文献
Simon; Salzbrunn; Surya Prakash; Petasis; Olah
Journal of Organic Chemistry, 2001 , vol. 66, # 2 p. 633 - 634
参考文献
Tomita
Yakugaku Zasshi, 1933 , vol. 53, p. 775,782; dtsch. Ref. S. 138
Chem. Zentralbl., 1933 , vol. 104, # II p. 3132
反应条件
potassium carbonate in acetonitrile T=50°C; 24 h; Overall yield = 67 percent; regioselective reaction;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
