N,N'-二邻甲苯基甲脒合成路线 (共 23 条)
反应条件
water; 2-(1,3-dioxoindan-2-ylidene)malononitrile 1.) EtOAc, RT, 1 h; Yield given. Multistep reaction;
参考文献
Doep, Dietrich; Gomaa, Mohsen A.; Henkel, Gerald; El-Din, Ahmed M. Nour
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 4 p. 573 - 576
反应条件
water 1.) EtOAc, RT, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Doep, Dietrich; Gomaa, Mohsen A.; Henkel, Gerald; El-Din, Ahmed M. Nour
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 4 p. 573 - 576
反应条件
β-cyclodextrin in ethanol; water
T=20°C; 12 h; Green chemistry; Catalytic behavior;
参考文献
Patil, Dipak R.; Dalal, Dipak S.
Chinese Chemical Letters, 2012 , vol. 23, # 10 p. 1125 - 1128
反应条件
choline chloride*2SnCl2
T=90°C;
参考文献
Azizi, Najmadin; Gholibeglo, Elham; Babapour, Mahbobe; Ghafuri, Hossein; Bolourtchian, Seyed Mohammad
Comptes Rendus Chimie, 2012 , vol. 15, # 9 p. 768 - 773
反应条件
orthoformic acid triethyl ester
T=140°C;
参考文献
Kuhn, Kevin M.; Grubbs, Robert H.
Organic Letters, 2008 , vol. 10, # 10 p. 2075 - 2077
反应条件
sodium hydroxide; trimethylsilyl bromide in dichloromethane
T=0°C;
参考文献
Oehme, Hartmut; Wustrack, Ronald
Zeitschrift fuer Chemie (Stuttgart, Germany), 1983 , vol. 23, # 10 p. 374
反应条件
1: With ethanesulfonic acid in tetrahydrofuran
24 h; Inert atmosphereHeating;
2: With potassium carbonate in dichloromethane
Inert atmosphere;
参考文献
Tam, Annie; Armstrong, Ian S.; La Cruz, Thomas E.
Organic Letters, 2013 , vol. 15, # 14 p. 3586 - 3589
反应条件
sodium tetrahydroborate in isopropyl alcohol
参考文献
Kaji,K. et al.
Chemical and Pharmaceutical Bulletin, 1978 , vol. 26, p. 2246 - 2249
参考文献
Roberts et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 2277,2281
参考文献
Ladenburg
Chemische Berichte, 1877 , vol. 10, p. 1260