1,2-二氢-1-苯基萘合成路线 (共 25 条)
反应条件
HZSM-5 zeolite in 2,2,4-trimethylpentane
T=20°C; 2 h; Irradiation; Product distribution; Further Variations:ReagentsSolventsother substrates;
参考文献
Ikeda, Hiroshi; Nomura, Tsuyoshi; Akiyama, Kimio; Oshima, Mitsuhiro; Roth, Heinz D.; Tero-Kubota, Shozo; Miyashi, Tsutomu
Journal of the American Chemical Society, 2005 , vol. 127, # 41 p. 14497 - 14504
反应条件
1: 7.6 g / polyphosphoric acid / 1 h / 90 °C
2: 4.8 g / sodium borohydride / ethanol
3: 70 percent / phosphoric acid / 2 h / 120 - 130 °C
View Scheme
参考文献
Kopecky, Karl R.; Hall, Michael C.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 3095 - 3104
反应条件
in water
T=80°C; 24 h; Sealed tube; optical yield given as percent ee;
参考文献
Vincek, Adam S.; Booth, Raymond G.
Tetrahedron Letters, 2009 , vol. 50, # 36 p. 5107 - 5109
反应条件
2,4,6-triphenylpyrylium-tetrafluoroborate in dichloromethane
0.833333 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Mlcoch, Jiri; Steckhan, Eberhard
Angewandte Chemie, 1985 , vol. 97, # 5 p. 429 - 431
反应条件
T=500 - 900°C; P=0.1 Torr; Product distributionMechanism;
参考文献
Lamberts, Joseph J.; Laarhoven, Wim H.
Journal of Organic Chemistry, 1984 , vol. 49, # 1 p. 100 - 106
反应条件
T=900°C; P=0.1 Torr; flash vacuum pyrolysis; Title compound not separated from byproducts;
参考文献
Lamberts, Joseph J. M.; Cuppen, Theo J. H. M.; Laarhoven, Wim H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1819 - 1828
反应条件
aluminum tri-bromide
T=60°C; 0.5 h; Sonication;
参考文献
Golounin; Marakushina; Khramenko
Russian Journal of Applied Chemistry, 2008 , vol. 81, # 12 p. 2137 - 2140
反应条件
in benzene
T=84°C; 72 h; Product distributionMechanism;
参考文献
Kopecky, Karl R.; Hall, Michael C.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 3095 - 3104
反应条件
T=500 - 900°C; P=0.1 Torr; Product distributionMechanism;
参考文献
Lamberts, Joseph J.; Laarhoven, Wim H.
Journal of Organic Chemistry, 1984 , vol. 49, # 1 p. 100 - 106
参考文献
Voigtlaender; Rosenberg
Archiv der Pharmazie (Weinheim, Germany), 1959 , vol. 292, p. 632,641