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(1-萘)三氟硼酸钾
合成路线
（共 26 条）
13922-41-3
1-萘硼酸
→
反应条件
166328-07-0
(1-萘)三氟硼酸钾
反应条件
1: With potassium fluoride in water; acetonitrile T=21°C; 2: With L-(+)-tartaric acid in tetrahydrofuran; water; acetonitrile
参考文献
Lennox, Alastair J. J.; Lloyd-Jones, Guy C.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 37 p. 9385 - 9388
38262-42-9
→
反应条件
166328-07-0
(1-萘)三氟硼酸钾
反应条件
1: With tetrahydroxydiboron; [1,3-bis(diphenylphosphino) propane] dichloronickel(II); N-ethyl-N,N-diisopropylamine; triphenylphosphine in ethanol T=50°C; Miyaura Borylation Reaction; 8 h; Inert atmosphereSealed tube; 2: With potassium hydrogen difluoride in methanol; ethanol; water T=0 - 20°C; 0.5 h;
参考文献
Molander, Gary A.; Cavalcanti, Livia N.; Garcia-Garcia, Carolina
Journal of Organic Chemistry, 2013 , vol. 78, # 13 p. 6427 - 6439
166328-07-0
(1-萘)三氟硼酸钾
→
反应条件
321-38-0
1-氟萘
反应条件
2,2-dimethyl-1-propanenitrile; 1-Fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; [Cu(CH3CN)4]BF4 in ethyl acetate T=80°C; 12 h; Inert atmosphereGlovebox;
参考文献
Ye, Yingda; Sanford, Melanie S.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4648 - 4651
166328-07-0
(1-萘)三氟硼酸钾
→
反应条件
91-20-3
萘
+
321-38-0
1-氟萘
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile T=20°C; 24 h; Inert atmosphere;
参考文献
Cazorla, Clement; Metay, Estelle; Andrioletti, Bruno; Lemaire, Marc
Tetrahedron Letters, 2009 , vol. 50, # 27 p. 3936 - 3938
75-05-8
乙腈
+
166328-07-0
(1-萘)三氟硼酸钾
→
反应条件
941-98-0
1-乙酰基萘
反应条件
[2,2']bipyridinyl; palladium (II) trifluoroacetate; water; trifluoroacetic acid in tetrahydrofuran T=80°C; 36 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Xingyong; Liu, Miaochang; Xu, Long; Wang, Qingzong; Chen, Jiuxi; Ding, Jinchang; Wu, Huayue
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5273 - 5281
166328-07-0
(1-萘)三氟硼酸钾
→
反应条件
90-14-2
1-碘萘
反应条件
chloramine-T; sodium iodide in tetrahydrofuran; water T=20°C; 0.166667 h;
参考文献
Kabalka, George W.; Mereddy, Arjun R.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 343 - 345
166328-07-0
(1-萘)三氟硼酸钾
→
反应条件
90-13-1
α-氯代萘
反应条件
trichloroisocyanuric acid in water; ethyl acetate T=20°C; 0.666667 h; Open flask;
参考文献
Molander, Gary A.; Cavalcanti, Livia N.
Journal of Organic Chemistry, 2011 , vol. 76, # 17 p. 7195 - 7203
626-60-8
3-氯吡啶
+
166328-07-0
(1-萘)三氟硼酸钾
→
反应条件
189193-21-3
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium carbonate; palladium diacetate in methanol T=67°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Barder, Timothy E.; Buchwald, Stephen L.
Organic Letters, 2004 , vol. 6, # 16 p. 2649 - 2652
108-86-1
溴代苯
+
166328-07-0
(1-萘)三氟硼酸钾
→
反应条件
605-02-7
1-苯基萘
反应条件
potassium carbonate; triphenylphosphine in methanol T=50°C; Suzuki-Miyaura coupling; 24 h;
参考文献
Masuyama, Yoshiro; Sugioka, Yutaka; Chonan, Shiori; Suzuki, Noriyuki; Fujita, Masahiro; Hara, Kenji; Fukuoka, Atsushi
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 352, p. 81 - 85
166328-07-0
(1-萘)三氟硼酸钾
→
反应条件
90-15-3
1-萘酚
反应条件
Oxonereg;; water in acetone T=20°C; 0.0333333 h;
参考文献
Molander, Gary A.; Cavalcanti, Livia N.
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 623 - 630
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