3-(3-硝基苯基)败脂酸甲基酯合成路线 (共 12 条)
反应条件
hydrogen; palladium on activated charcoal
参考文献
Hashizume; Ito; Morikawa; Kanaya; Nagashima; Usui; Tomoda; Sunazuka; Kumagai; Omura
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 10 p. 2097 - 2107
反应条件
sulfuric acid
24 h; Reflux;
参考文献
Pinto, Orlando; Sardinha, Joao; Vaz, Pedro D.; Piedade, Fatima; Calhorda, Maria J.; Abramovitch, Rudolph; Nazareth, Nair; Pinto, Madalena; Nascimento, Maria S. J.; Rauter, Amelia P.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 9 p. 3175 - 3187
反应条件
tributyl-amine in N-dodecane
T=120°C; Heck reaction; 3 h;
参考文献
Jung, Ji-Young; Taher, Abu; Kim, Hyun-Jin; Ahn, Wha-Seung; Jin, Myung-Jong
Synlett, 2009 , # 1 p. 39 - 42
反应条件
nano-FeDOPAPd catalyst in water
Heck Reaction; Sonication;
参考文献
Nasir Baig; Varma, Rajender S.
Green Chemistry, 2013 , vol. 15, # 2 p. 398 - 417
反应条件
dilithium tetrachloropalladate
参考文献
Heck,R.F.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5518 - 5526
反应条件
sodium methylate
1.) methanol, 10 min, 2.) methanol, RT, 1 h; Multistep reaction;
参考文献
Hashizume; Ito; Morikawa; Kanaya; Nagashima; Usui; Tomoda; Sunazuka; Kumagai; Omura
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 10 p. 2097 - 2107
反应条件
1.1: silica-gel-supported sulfuric acid; sodium nitrite / |Milling
1.2: |Milling
2.1: potassium carbonate / 1.2 h / 130 °C / |Green chemistry
View Scheme
参考文献
Hajipour, Abdol Reza; Azizi, Ghobad
Green Chemistry, 2013 , vol. 15, # 4 p. 1030 - 1034
参考文献
Asunskis,J.; Shechter,H.
Journal of Organic Chemistry, 1968 , vol. 33, # 3 p. 1164 - 1168
参考文献
Asunskis,J.; Shechter,H.
Journal of Organic Chemistry, 1968 , vol. 33, # 3 p. 1164 - 1168
反应条件
reagiert analog mit anderen aromatischen Aldehyden;
参考文献
Galat
Journal of the American Chemical Society, 1946 , vol. 68, p. 376