1: N,N-diisobutyl-2,4-dimethyl-3-pentylamine / CH2Cl2 / 12 h / 0 °C
2: MgI2 / CS2 / 2 h / 0 °C
3: DBU / 0.33 h / 100 °C
View Scheme
参考文献
Martinez, A. Garcia; Alvarez, R. Martinez; Gonzalez, S. Martinez; Subramanian, L. R.; Conrad, M.
Tetrahedron Letters, 1992 , vol. 33, # 15 p. 2043 - 2044
1: MgI2 / CS2 / 2 h / 0 °C
2: DBU / 0.33 h / 100 °C
View Scheme
参考文献
Martinez, A. Garcia; Alvarez, R. Martinez; Gonzalez, S. Martinez; Subramanian, L. R.; Conrad, M.
Tetrahedron Letters, 1992 , vol. 33, # 15 p. 2043 - 2044
1,8-diazabicyclo[5.4.0]undec-7-ene
T=100°C; 0.333333 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Martinez, A. Garcia; Alvarez, R. Martinez; Gonzalez, S. Martinez; Subramanian, L. R.; Conrad, M.
Tetrahedron Letters, 1992 , vol. 33, # 15 p. 2043 - 2044
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Basavaiah, Deevi; Kulkarni, Surendra U.; Bhat, Narayan G.; Prasad, J. V. N. Vara
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 239 - 246
