反应条件
1: 95 percent / sodium borohydride / ethanol / 4 h / 58 °C
2: 79 percent / hydrochloric acid, water / 4.5 h / 50 °C
3: 17 percent / 1.) n-butyl-lithium, 2.) n-butyl-lithium / 1.) -30 deg C, 1h, 2.) -30 - -25 deg C, 30 min
View Scheme
参考文献
Adlington, Robert M.; Barrett, Anthony G. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2848 - 2863