2′,4′,6′-三甲基苯乙酮合成路线 （共 135 条）
反应条件
oxygen; palladium diacetate; trifluoroacetic acid in water; dimethyl sulfoxide T=70°C; Wacker Oxidation; P=760.051 Torr; 10 h; Sealed tube; regioselective reaction;
参考文献
Wang, Yu-Fei; Gao, Ya-Ru; Mao, Shuai; Zhang, Yan-Lei; Guo, Dong-Dong; Yan, Zhao-Lei; Guo, Shi-Huan; Wang, Yong-Qiang
Organic Letters, 2014 , vol. 16, # 6 p. 1610 - 1613
反应条件
indium trifluoromethanesulfonate; lithium perchlorate in nitromethane T=20°C;
参考文献
Chapman, Christopher J.; Frost, Christopher G.; Hartley, Joseph P.; Whittle, Alan J.
Tetrahedron Letters, 2001 , vol. 42, # 5 p. 773 - 775
反应条件
tetrabutylammomium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dichloromethane; water T=20°C; 4 h;
参考文献
Kuhakarn, Chutima; Kittigowittana, Krisada; Ghabkham, Pattama; Pohmakotr, Manat; Reutrakul, Vichai
Synthetic Communications, 2006 , vol. 36, # 19 p. 2887 - 2892
反应条件
iron(III) oxide T=20°C; Friedel Crafts acylation; 0.166667 h; regioselective reaction;
参考文献
Sharghi, Hashem; Jokar, Mahboubeh; Doroodmand, Mohammad Mahdi; Khalifeh, Reza
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 3031 - 3044
反应条件
HFBAA T=100°C; Friedel-Crafts acetylation; 3 h;
参考文献
Matsushita, Yoh-Ichi; Sugamoto, Kazuhiro; Matsui, Takanao
Tetrahedron Letters, 2004 , vol. 45, # 24 p. 4723 - 4727
反应条件
sodium hydrogencarbonate; sodium bromide; chiral azabicyclo-N-oxyl in dichloromethane T=0°C; Electrochemical reaction;
参考文献
Shiigi, Hirofumi; Mori, Hiroyuki; Tanaka, Tomoaki; Demizu, Yosuke; Onomura, Osamu
Tetrahedron Letters, 2008 , vol. 49, # 36 p. 5247 - 5251
反应条件
tert.-butyl lithium in tetrahydrofuran T=25°C; 0.25 h;
参考文献
Gokhale, Abha; Schiess, Peter
Helvetica Chimica Acta, 1998 , vol. 81, # 2 p. 251 - 267
反应条件
diethyl ether; nickel T=150 - 160°C; P=110326 - 147102 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 57, p. 143,145
反应条件
trifluoroacetic acid in dimethyl sulfoxide T=70°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 126, # 8 p. 2302 - 2303
反应条件
1: With dimethyl sulfoxide; trifluoroacetic acid; palladium diacetate T=80°C; 24 h; 2: With water T=70°C; 2 h;
参考文献
Zhou, Chengxiang; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3551 - 3558
