5-(4-硝基苯基)-1H-四唑合成路线 （共 29 条）
反应条件
T=170°C; 0.5 h; Microwave irradiation;
参考文献
Efimova; Karabanovich; Artamonova; Koldobskii
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 4 p. 631 - 632
反应条件
dicyclohexyl-carbodiimide in toluene
T=120°C; 0.25 h;
参考文献
Povazanec, Frantisek; Kovac, Jaroslav; Svoboda, Jozef
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 4 p. 1299 - 1300
反应条件
T=100°C; 1 h; Microwave irradiation;
参考文献
Efimova; Artamonova; Koldobskii
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 9 p. 1345 - 1347
参考文献
Jursic; Zdravkovski
Synthetic Communications, 1994 , vol. 24, # 11 p. 1575 - 1582
参考文献
Huisgen,R. et al.
Chemische Berichte, 1960 , vol. 93, p. 2106 - 2124
反应条件
dicyclohexyl-carbodiimide in toluene
T=120°C; 0.25 h;
参考文献
Povazanec, Frantisek; Kovac, Jaroslav; Svoboda, Jozef
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 4 p. 1299 - 1300
反应条件
sodium hydride in N,N-dimethyl-formamide
T=0 - 20°C;
参考文献
Bristol-Myers Squibb Pharma Company
Patent: EP946508 B1, 2009 ;
Location in patent: Page/Page column 53 ;
反应条件
sodium hydride in N,N-dimethyl-formamide
T=5°C; 1.5 h;
参考文献
GALAPAGOS N.V.
Patent: WO2007/131991 A1, 2007 ;
Location in patent: Page/Page column 82-83 ;
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane
T=25°C; 5 h; Product distribution;
参考文献
Osipova, T. F.; Ostrovskii, V. A.; Koldobskii, G. I.; Erusalimskii, G. B.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 357 - 362
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 398 - 404
