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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-异丁基萘
合成路线
（共 15 条）
63942-77-8
+
90-11-9
1-溴代萘
→
反应条件
16727-91-6
1-异丁基萘
反应条件
sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; water 16 h; Heating;
参考文献
Miyaura, Norio; Ishiyama, Tatsuo; Sasaki, Hirotomo; Ishikawa, Masako; Satoh, Makoto; Suzuki, Akira
Journal of the American Chemical Society, 1989 , vol. 111, # 1 p. 314 - 321
1144-13-4
+
5674-02-2
异丁基氯化镁
→
反应条件
16727-91-6
1-异丁基萘
反应条件
N,N'-di(2,4,6-trimethylphenyl)-4,5-dihydroimidazolinium chloride; iron(II) chloride in tetrahydrofuran; dichloromethane T=65°C; 3 h; Inert atmosphereSealed tube;
参考文献
Silberstein, Amanda L.; Ramgren, Stephen D.; Garg, Neil K.
Organic Letters, 2012 , vol. 14, # 14 p. 3796 - 3799
85630-39-3
+
5674-02-2
异丁基氯化镁
→
反应条件
16727-91-6
1-异丁基萘
反应条件
N,N'-di(2,4,6-trimethylphenyl)-4,5-dihydroimidazolinium chloride; iron(II) chloride in tetrahydrofuran; dichloromethane T=65°C; 3 h; Inert atmosphereSealed tube;
参考文献
Silberstein, Amanda L.; Ramgren, Stephen D.; Garg, Neil K.
Organic Letters, 2012 , vol. 14, # 14 p. 3796 - 3799
54125-11-0
→
反应条件
16727-91-6
1-异丁基萘
反应条件
1: 97 percent / xylene / 72 h / Heating 2: tert-butyllithium / 1.) THF, pentane, room temperature, 2.) 1 h 3: 95 percent / hydrogen / 10percent palladium on carbon / methanol / 3 h View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
24973-91-9
→
反应条件
16727-91-6
1-异丁基萘
反应条件
1: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 4.5 h / Heating 2: 97 percent / xylene / 72 h / Heating 3: tert-butyllithium / 1.) THF, pentane, room temperature, 2.) 1 h 4: 95 percent / hydrogen / 10percent palladium on carbon / methanol / 3 h View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
85924-73-8
→
反应条件
16727-91-6
1-异丁基萘
反应条件
1: 25 mg / tetrahydrofuran / 0.17 h / -78 °C 2: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 4.5 h / Heating 3: 97 percent / xylene / 72 h / Heating 4: tert-butyllithium / 1.) THF, pentane, room temperature, 2.) 1 h 5: 95 percent / hydrogen / 10percent palladium on carbon / methanol / 3 h View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
85924-89-6
→
反应条件
16727-91-6
1-异丁基萘
反应条件
1: tert-butyllithium / 1.) THF, pentane, room temperature, 2.) 1 h 2: 95 percent / hydrogen / 10percent palladium on carbon / methanol / 3 h View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
85864-98-8
→
反应条件
16727-91-6
1-异丁基萘
反应条件
1: 15 percent / tetrahydrofuran / 48 h / Heating 2: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 4.5 h / Heating 3: 97 percent / xylene / 72 h / Heating 4: tert-butyllithium / 1.) THF, pentane, room temperature, 2.) 1 h 5: 95 percent / hydrogen / 10percent palladium on carbon / methanol / 3 h View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
90-11-9
1-溴代萘
→
反应条件
16727-91-6
1-异丁基萘
反应条件
triphenylphosphine; [(CO)4Fe(μ-PPh2)Pd(μ-Cl)]2 in benzene T=78°C; 4 h;
参考文献
Shenglof, Margarita; Gelman, Dmitri; Heymer, Bernd; Schumann, Herbert; Molander, Gary A.; Blum, Jochanan
Synthesis, 2003 , # 2 p. 302 - 306
90-11-9
1-溴代萘
+
115-11-7
异丁烯
→
反应条件
16727-91-6
1-异丁基萘
反应条件
sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride 1.) THF, r.t., 6 h; 2.) THF, 65 deg C, 16 h; Yield given. Multistep reaction;
参考文献
Miyaura, Norio; Ishiyama, Tatsuo; Sasaki, Hirotomo; Ishikawa, Masako; Satoh, Makoto; Suzuki, Akira
Journal of the American Chemical Society, 1989 , vol. 111, # 1 p. 314 - 321
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