Van Der Toorn, John C.; Kemperman, Gerjan; Sheldon, Roger A.; Arends, Isabel W. C. E.
European Journal of Organic Chemistry, 2011 , # 23 p. 4345 - 4352
1: tetrahydrofuran / 0.67 h / 20 - 25 °C / |Large scale
2: methanesulfonic acid; hydrogen bromide / n-heptane / 0.5 h / 65 - 75 °C / |Large scale
3: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / |Large scale
4: potassium carbonate / N,N-dimethyl-formamide; water / 35 °C / |Large scale
5: palladium on carbon; acetic acid / tetrahydrofuran / 60 °C / 1725.17 Torr / |Large scale
View Scheme
参考文献
Alorati, Anthony D.; Gibb, Andrew D.; Mullens, Peter R.; Stewart, Gavin W.
Organic Process Research and Development, 2012 , vol. 16, # 12 p. 1947 - 1952
