反应条件
2: 95 percent / 1) H2, 5percent palladium-carbon / 1) 95percent Ethanol, room temperature, 1 h, 2) Diethylether, cooling, overnight 3: 16 percent / 1) Oxalyl chloride / 0 °C / 1) methylene dichloride, 2) ether, 0.5 h 4: 88 percent / 1.0 N sodium hydroxide / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Pettit, George R.; Nelson, Paul S.
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 741 - 744