三(乙腈)三羰基铬(0)合成路线 （共 15 条）
反应条件
in cyclohexane boiling;;
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.6.1.2.1.1, page 183 - 190
反应条件
in diethyl ether at 0°C; (1)H NMR, mass spectrum;
参考文献
Reynolds, Stephen D.; Albright, T. A.
Organometallics, 1985 , vol. 4, p. 980 - 986
反应条件
in tetrahydrofuran under Ar; addn. of triene in THF to Cr-complex, kept (40°C, 18 h); filtration (SiO2), evapn., column chromy. (degassed silica, petroleum ether/diethyl ether);
参考文献
Berno, Piero; Ceccon, Alberto; Dapra, Francesca; Gambaro, Alessandro; Venzo, Alfonso; et al.
Journal of Organometallic Chemistry, 1986 , vol. 301, p. 161 - 172
反应条件
in anhydrous butyl ether treatment of tris(acetonitrile)tricarbonylmetal complex with benzene deriv. in n-Bu2O at 50°C in vac.; chromy. (silica gel), recrystn. from hexane/benzene or toluene;
参考文献
Mueller, Joern; Luedemann, Frerk
Journal of Organometallic Chemistry, 1981 , vol. 204, # 3 p. 361 - 376
反应条件
in anhydrous butyl ether
treatment of tris(acetonitrile)tricarbonylmetal complex with benzene deriv. in n-Bu2O at 50°C in vac.; chromy. (silica gel), recrystn. from hexane/benzene or toluene;
参考文献
Mueller, Joern; Luedemann, Frerk
Journal of Organometallic Chemistry, 1981 , vol. 204, # 3 p. 361 - 376
