三甲基-(三甲基锡烷基甲基)锡烷合成路线 （共 34 条）
反应条件
bromine in dichloromethane (N2); monitored by (1)H NMR;
参考文献
Hawker, Darryl W.; Wells, Peter R.
Organometallics, 1985 , vol. 4, p. 821 - 825
反应条件
in tetrachloromethane under N2 at 0°C; not isolated, detected by NMR;
参考文献
Kuivila, Henry G.; Karol, Thomas J.; Swami, Kamal
Organometallics, 1983 , vol. 2, p. 909 - 914
反应条件
iodine in chlorobenzene (N2); monitored by (1)H NMR;
参考文献
Hawker, Darryl W.; Wells, Peter R.
Organometallics, 1985 , vol. 4, p. 821 - 825
反应条件
Br2 in methanol; tetrachloromethane treatment with Br2 in MeOH/CCl4 at -60°C, warmed;
参考文献
Karol, Thomas J.; Hutchinson, John P.; Hyde, Jeffrey R.; Kuivila, Henry G.; Zubieta, Jon A.
Organometallics, 1983 , vol. 2, p. 106 - 114
反应条件
Yield given. Multistep reaction;
参考文献
Sato, Tadashi; Ariura, Shigeki
Angewandte Chemie, 1993 , vol. 105, # 1 p. 129 - 130
反应条件
Yield given. Multistep reaction;
参考文献
Sato, Tadashi; Ariura, Shigeki
Angewandte Chemie, 1993 , vol. 105, # 1 p. 129 - 130
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; methylene double anion donors, var. esters; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 53, # 6 p. 1207 - 1212
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Sato, Tadashi; Matsuoka, Hiroharu; Igarashi, Tsutomu; Minomura, Masafumi; Murayama, Eigoro
Journal of Organic Chemistry, 1988 , vol. 53, # 6 p. 1207 - 1212
反应条件
Na; CH2Cl2 in ammonia; pentane
NH3 (liquid); (N2); trimethylchlorostannane and pentane transferred into flask, NH3 condensed, stirred while Na added for 5 min, stirred for 10 min, CH2Cl2 added slowly with stirring; NH3 evapd., extd. with pentane and H2O, org. layer washed with aq. H2SO4, then with H2O, dried (MgSO4), filtered, concd., distd. (0.01 Torr) while being stirred at room temp.;
参考文献
Karol, Thomas J.; Hutchinson, John P.; Hyde, Jeffrey R.; Kuivila, Henry G.; Zubieta, Jon A.
Organometallics, 1983 , vol. 2, p. 106 - 114
反应条件
dichloromethane; sodium in ammonia
(N2); a soln. of (trimethylstannyl)sodium treated dropwise with CH2Cl2; treated with moist ether; titrated with a soln. of I2 in ether; washed with a soln. of Na2S2O5; dried; evapd.; distd.;
参考文献
Hawker, Darryl W.; Wells, Peter R.
Organometallics, 1985 , vol. 4, p. 821 - 825
