3,4-二苯基异苯并吡喃-1-酮合成路线 （共 25 条）
反应条件
silver(I) acetate in methanol
T=60°C; 24 h; Reagent/catalyst;
参考文献
Frasco, Daniel A.; Lilly, Cassandra P.; Boyle, Paul D.; Ison, Elon A.
ACS Catalysis, 2013 , vol. 3, # 10 p. 2421 - 2429
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; copper diacetate in 1,1-dimethylpropan-1-ol
T=110°C; 16 h;
参考文献
Hyster, Todd K.; Rovis, Tomislav
Journal of the American Chemical Society, 2010 , vol. 132, # 30 p. 10565 - 10569
反应条件
water; oxalic acid in tetrahydrofuran
T=60°C; 10 h; Inert atmosphere;
参考文献
Miura, Tomoya; Hiraga, Kentaro; Toyoshima, Takeharu; Yamauchi, Motoshi; Murakami, Masahiro
Chemistry Letters, 2012 , vol. 41, # 8 p. 798 - 800
反应条件
[(η5-C5Me5)2Rh2(μ-Cl)2Cl2]; silver(I) acetate in 2,2,2-trifluoroethanol
T=60°C; 16 h; Sealed tubeInert atmosphere; Catalytic behavior; Reagent/catalystSolventTemperature; regioselective reaction;
参考文献
Li, Xing Guang; Liu, Kai; Zou, Gang; Liu, Pei Nian
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 7 p. 1496 - 1500
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; copper diacetate in 1,1-dimethylpropan-1-ol
T=110°C; 16 h;
参考文献
Hyster, Todd K.; Rovis, Tomislav
Journal of the American Chemical Society, 2010 , vol. 132, # 30 p. 10565 - 10569
反应条件
1: 20 percent / xylene / 130 °C
2: silica, H2O
View Scheme
参考文献
Le Roux, Jean-Pierre; Desbene, Paul-Louis; Cherton, Jean-Claude
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 847 - 849
反应条件
1: triethylamine / dichloromethane / 15.5 h / 20 °C / Inert atmosphere
2: bis(1,5-cyclooctadiene)nickel (0); potassium carbonate; tris(p-chloro phenyl)phosphine / toluene / 17 h / 80 °C / Inert atmosphere
3: water; oxalic acid / tetrahydrofuran / 10 h / 60 °C / Inert atmosphere
View Scheme
参考文献
Miura, Tomoya; Hiraga, Kentaro; Toyoshima, Takeharu; Yamauchi, Motoshi; Murakami, Masahiro
Chemistry Letters, 2012 , vol. 41, # 8 p. 798 - 800
反应条件
1: bis(1,5-cyclooctadiene)nickel (0); potassium carbonate; tris(p-chloro phenyl)phosphine / toluene / 17 h / 80 °C / Inert atmosphere
2: water; oxalic acid / tetrahydrofuran / 10 h / 60 °C / Inert atmosphere
View Scheme
参考文献
Miura, Tomoya; Hiraga, Kentaro; Toyoshima, Takeharu; Yamauchi, Motoshi; Murakami, Masahiro
Chemistry Letters, 2012 , vol. 41, # 8 p. 798 - 800
反应条件
1: triethylamine / dichloromethane / 0.67 h / 20 °C / |Inert atmosphere; |Schlenk technique
2: [(η5-C5Me5)2Rh2(μ-Cl)2Cl2]; silver(I) acetate / 2,2,2-trifluoroethanol / 16 h / 60 °C / |Sealed tube; |Inert atmosphere
View Scheme
参考文献
Li, Xing Guang; Liu, Kai; Zou, Gang; Liu, Pei Nian
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 7 p. 1496 - 1500
反应条件
water; silica gel
Yield given;
参考文献
Le Roux, Jean-Pierre; Desbene, Paul-Louis; Cherton, Jean-Claude
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 847 - 849
