反应条件
in neat (no solvent) byproducts: NaCN, CO2, NH3; High Pressure; mixing of NaBH4 and CO(NH2)2, placing into stainless steel autoclave, sealing and heating at rate of 20°C/min in furnace to 550°C,heating at this temp. for 10 h, natural cooling to ambient temp.; washing with EtOH, dilute HCl and H2O several times, drying at 60°C for 10 h;
参考文献
Meng, Xiang-Lin; Lun, Ning; Qi, Yong-Xin; Zhu, Hui-Ling; Han, Fu-Dong; Yin, Long-Wei; Fan, Run-Hua; Bai, Yu-Jun; Bi, Jian-Qiang
Journal of Solid State Chemistry, 2011 , vol. 184, # 4 p. 859 - 862
