N,N-二乙基苯甲酰胺合成路线 (共 244 条)
反应条件
1: iodobenzene; diethylamine With sodium carbonate in water 0.166667 h; Autoclave; 2: carbon dioxide in water T=100°C; P=5171.62 Torr; 8 h; Autoclave;
参考文献
Qureshi, Ziyauddin S.; Revankar, Santosh A.; Khedkar, Mayur V.; Bhanage, Bhalchandra M.
Catalysis Today, 2012 , vol. 198, # 1 p. 148 - 153
反应条件
triethylamine in dichloromethane T=20°C; 0.333333 h;
参考文献
Barbe, Guillaume; Charette, Andre B.
Journal of the American Chemical Society, 2008 , vol. 130, # 1 p. 18 - 19
反应条件
carbon monoxide; (dipp)2Pd(O) in xylene T=150°C; P=3620.04 Torr; 20 h;
参考文献
Ben-David, Yehoshua; Portnoy, Moshe; Milstein, David
Journal of the American Chemical Society, 1989 , vol. 111, # 23 p. 8742 - 8744
反应条件
bis(trimethylaluminum)-1,4-diazabicyclo[2.2.2]octane in tetrahydrofuran T=130°C; 0.133333 h; Inert atmosphereMicrowave irradiation;
参考文献
Dubois, Nathalie; Glynn, Daniel; McInally, Thomas; Rhodes, Barrie; Woodward, Simon; Irvine, Derek J.; Dodds, Chris
Tetrahedron, 2013 , vol. 69, # 46 p. 9890 - 9897
反应条件
imidazole hydrochloride in water T=20°C; 0.166667 h;
参考文献
Verma, Sanjeev K.; Ghorpade, Ramarao; Pratap, Ajay; Kaushik
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2373 - 2376
反应条件
tert.-butylhydroperoxide; iron(II) chloride in decane; acetonitrile T=85°C; 1 h; Schlenk techniqueInert atmosphere;
参考文献
Li, Yuanming; Jia, Fan; Li, Zhiping
Chemistry - A European Journal, 2013 , vol. 19, # 1 p. 82 - 86
反应条件
N-ethyl-N,N-diisopropylamine; [bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane T=0°C; 0.5 h;
参考文献
Kangani, Cyrous O.; Kelley, David E.
Tetrahedron Letters, 2005 , vol. 46, # 51 p. 8917 - 8920
反应条件
sodium hypochlorite; tetra(n-butyl)ammonium hydrogensulfate T=120°C; 12 h;
参考文献
Liang, Jun; Lv, Jing; Shang, Zhi-Cai
Tetrahedron, 2011 , vol. 67, # 44 p. 8532 - 8535
反应条件
(Ph3P)2Pd(Ph)(I) T=120°C; 64 h;
参考文献
Kobayashi, Toshiaki; Tanaka, Masato
Journal of Organometallic Chemistry, 1982 , vol. 231, # 1 p. C12 - C14
反应条件
tributyl-amine T=20°C; 0.333333 h;
参考文献
DIRECTOR GENERAL, DEFENCE RESEARCH and DEVELOPMENT ORGANISATION; RAO, Ambati Narasimha; GANESAN, Kumaran; VIJAYARAGHAVAN, Rajagopalan
Patent: WO2013/65059 A1, 2013 ;
Location in patent: Page/Page column 13; 14 ;