N,N-二乙基苯甲酰胺合成路线 （共 244 条）
反应条件
water 1) hexane, 20 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Kalikhman, I. D.; Vyazankina, O. A.; Vyazankin, N. S.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1838 - 1843,1654 - 1658
反应条件
dimethylsulfide borane complex in toluene 4 h; Heating;
参考文献
Kuwano, Ryoichi; Takahashi, Masatoshi; Ito, Yoshihiko
Tetrahedron Letters, 1998 , vol. 39, # 9 p. 1017 - 1020
反应条件
Li-n-BuBH3 in hexane; toluene T=25°C; 24 h; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 47, # 17 p. 3311 - 3315
反应条件
thionyl chloride Destillieren des Reaktionsprodukts unter vermindertem Druck;
参考文献
v. Braun; Pinkernelle
Chemische Berichte, 1934 , vol. 67, p. 1218
参考文献
v. Braun
Chemische Berichte, 1904 , vol. 37, p. 2816
反应条件
Destillieren des Reaktionsprodukts unter vermindertem Druck;
参考文献
v. Braun; Pinkernelle
Chemische Berichte, 1934 , vol. 67, p. 1218
反应条件
1: s-BuLi; TMEDA / tetrahydrofuran 2: 93 percent / LDA / tetrahydrofuran / -10 - 20 °C View Scheme
参考文献
Pradhan, Tarun Kanti; De, Asish; Mortier, Jacques
Tetrahedron, 2005 , vol. 61, # 38 p. 9007 - 9017
反应条件
sec-BuLi in tetrahydrofuran; cyclohexane
参考文献
Air Products and Chemicals, Inc.
Patent: US5233074 A1, 1993 ;
反应条件
N,N,N',N,-tetramethylethylenediamine; Davis reagent; sec.-butyllithium 1) THF, cyclohexane, -78 deg C, 1 h, 2) to room temperature, 12 h; Yield given. Multistep reaction;
参考文献
De Silva; Reed; Billedeau; Wang; Norris; Snieckus
Tetrahedron, 1992 , vol. 48, # 23 p. 4863 - 4878
反应条件
oxygen; nitrogen(IV) oxide; ozone in 1,2-dichloro-ethane T=0°C; 7 h; Product distribution;
参考文献
Suzuki, Hitomi; Tomaru, Jun-ichiro; Murashima, Takashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2413 - 2416
