N,N-二乙基苯甲酰胺合成路线 (共 244 条)
反应条件
manganese(IV) oxide; sodium cyanide in tetrahydrofuran T=20°C; 24 h;
参考文献
Foot, Jonathan S.; Kanno, Hisashi; Giblin, Gerard M. P.; Taylor, Richard J. K.
Synthesis, 2003 , # 7 p. 1055 - 1064
反应条件
N-dodecane; carbon monoxide; PdCl2(PMePh2)2 in toluene under CO (30 bars), 100 °C, 70 h; analysed by GC;
参考文献
Journal of Molecular Catalysis, , vol. 51, p. L15 - L20
反应条件
iodine; sodium hydroxide in water T=60°C; 4 h;
参考文献
Ding, Jiaoyang; Cao, Liping; Wang, Jungang; Xue, Weijian; Zhu, Yanping; Wu, Anxin
Journal of Chemical Research, 2011 , vol. 35, # 5 p. 298 - 301
反应条件
(Ph3P)2Pd(Ph)(I) in triethylamine T=120°C; P=15200 Torr; 44 h;
参考文献
Tetrahedron Letters, , vol. 27, # 39 p. 4745 - 4748
反应条件
1: phenyllithium With CuCN in diethyl ether T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in diethyl ether T=-30 - 20°C; 2 h;
参考文献
Organic Letters, , vol. 6, # 21 p. 3703 - 3706
反应条件
1-methyl-pyrrolidin-2-one; platinum(IV) oxide; sodium acetate T=70°C; 1 h;
参考文献
Hamze, Abdallah; Provot, Olivier; Alami, Mouad; Brion, Jean-Daniel
Organic Letters, 2006 , vol. 8, # 5 p. 931 - 934
反应条件
copper(I) oxide; 1,10-phenanthroline in 1-methyl-pyrrolidin-2-one; quinoline T=170°C; 12 h; Product distribution;
参考文献
Goossen, Lukas J.; Thiel, Werner R.; Rodriguez, Nuria; Linder, Christophe; Melzer, Bettina
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 14-15 p. 2241 - 2246
反应条件
tri(n-propyl)amine; tetraethylammonium chloride in diethylene glycol dimethyl ether T=150°C; 4 h; Inert atmosphere;
参考文献
Ren, Wei; Yamane, Motoki
Journal of Organic Chemistry, 2010 , vol. 75, # 24 p. 8410 - 8415
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trichlorophosphate T=135°C; 6 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Wagh, Yogesh S.; Bhatte, Kushal D.; Bhanage, Bhalchandra M.
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5489 - 5494
反应条件
4-(N,N-dimethlyamino)pyridine in diethyl ether 12 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 45, p. 4162 - 4167