1-环己烯基-苯基-甲酮合成路线 （共 47 条）
反应条件
ethanol; diethylamine
参考文献
Larramona
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1952 , vol. 235, p. 66
反应条件
potassium fluoride; 18-crown-6 ether; zinc(II) iodide in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=25°C; 24 h;
参考文献
Larson, Gerald L.; Prieto, Jose A.; Valle, Luis del
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1405 - 1412
反应条件
sulfuric acid; hydroquinone in chloroform
6 h; Ambient temperature;
参考文献
Ohta; Yamashita; Arita; Kajiura; Kawasaki; Noda; Izumi
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 8 p. 1294 - 1301
反应条件
1: 86 percent / aq. sodium acetate / 2 h / Ambient temperature
2: 79 percent / trifluoromethanesulfonic acid / CH2Cl2 / 16 h / Ambient temperature
View Scheme
参考文献
Olah, George A.; Wu, An-hsiang
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2531 - 2534
反应条件
1: 1. LDA / 1. THF, cyclohexane, -78 deg C, 30 min, 2a. 30 min, 2b. RT, overnight
2: 86 percent / aq. sodium acetate / 2 h / Ambient temperature
3: 79 percent / trifluoromethanesulfonic acid / CH2Cl2 / 16 h / Ambient temperature
View Scheme
参考文献
Olah, George A.; Wu, An-hsiang
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2531 - 2534
反应条件
1: in diethyl ether
Reflux;
2: With sulfuric acid; water
Reflux;
参考文献
Nakhai, Azadeh; Bergman, Jan
Tetrahedron, 2009 , vol. 65, # 11 p. 2298 - 2306
反应条件
copper(I) oxide; copper trifluoromethanesulfonate in acetonitrile
T=25°C; 0.5 h;
参考文献
Snider, Barry B.; Kwon, Taesoo
Journal of Organic Chemistry, 1992 , vol. 57, # 8 p. 2399 - 2410
反应条件
boron trifluoride diethyl etherate in dichloromethane
参考文献
Fujiwara, Jun; Watanabe, Masami; Sato, Tadashi
Journal of the Chemical Society, Chemical Communications, 1994 , # 3 p. 349 - 352
反应条件
1: SOCl2
2: H2O
3: diethyl ether / Heating
View Scheme
参考文献
Klein,J.
Tetrahedron, 1964 , vol. 20, p. 465 - 479
反应条件
1: H2O
2: diethyl ether / Heating
View Scheme
参考文献
Klein,J.
Tetrahedron, 1964 , vol. 20, p. 465 - 479
