1,2,3,4-四氢-1H-芴合成路线 （共 29 条）
反应条件
1.1: butyllithium; diisopropylamine / hexane; tetrahydrofuran / -78 - -20 °C
1.2: 80 percent / tetrahydrofuran / -78 - 20 °C
2.1: 74 percent / chromium(II) chloride; nickel cloride / dimethylformamide
3.1: 87 percent / p-toluenesulfonic acid / benzene / Heating
View Scheme
参考文献
Halterman, Ronald L.; Zhu, Chengian
Tetrahedron Letters, 1999 , vol. 40, # 42 p. 7445 - 7448
反应条件
1.1: butyllithium; diisopropylamine / hexane; tetrahydrofuran / -78 - -20 °C
1.2: 80 percent / tetrahydrofuran / -78 - 20 °C
2.1: 74 percent / chromium(II) chloride; nickel cloride / dimethylformamide
3.1: 87 percent / p-toluenesulfonic acid / benzene / Heating
View Scheme
参考文献
Halterman, Ronald L.; Zhu, Chengian
Tetrahedron Letters, 1999 , vol. 40, # 42 p. 7445 - 7448
反应条件
1: (i), (ii) Na, (iii) /BRN= 969135/
2: P2O5 / xylene / Heating
View Scheme
参考文献
Yakhontov,L.N. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1961 , vol. 31, # 10 p. 3190 - 3197,2977 - 2982
反应条件
2: P2O5 / xylene / Heating
View Scheme
参考文献
Yakhontov,L.N. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1961 , vol. 31, # 10 p. 3190 - 3197,2977 - 2982
反应条件
2: P2O5 / xylene / Heating
View Scheme
参考文献
Yakhontov,L.N. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1961 , vol. 31, # 10 p. 3190 - 3197,2977 - 2982
反应条件
2: aq. HBr
View Scheme
参考文献
Parham,W.E.; Sayed,Y.A.
Synthesis, 1976 , p. 116 - 117
反应条件
acetic acid; potassium iodide
参考文献
Treibs; Heyner
Chemische Berichte, 1957 , vol. 90, p. 2285,2290
反应条件
lithium aluminium tetrahydride; diethyl ether
Erhitzen des Reaktionsprodukts mit KHSO4;
参考文献
Christol et al.
Bulletin de la Societe Chimique de France, 1958 , p. 248,254
参考文献
Colonge; Sibeud
Bulletin de la Societe Chimique de France, 1953 , p. 75,76
