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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
17081-24-2
合成路线
（共 8 条）
106-39-8
4-溴氯苯
→
反应条件
17081-24-2
+
108-90-7
氯苯
+
71-43-2
苯
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 0.25 h; Irradiation; Title compound not separated from byproducts;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 885 - 886
6498-44-8
→
反应条件
17081-24-2
+
286-60-2
双环[6.1.0]壬烷
+
24266-07-7
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 8 h; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 885 - 886
2415-80-7
(2,2-二氯环丙基)苯
→
反应条件
17081-24-2
+
873-49-4
环丙基苯
+
17651-00-2
+
17650-99-6
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 8 h; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 885 - 886
5685-42-7
→
反应条件
17081-24-2
+
4468-61-5
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 8 h; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 885 - 886
1196-95-8
→
反应条件
17081-24-2
+
286-60-2
双环[6.1.0]壬烷
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 0.5 h; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 885 - 886
2415-79-4
→
反应条件
17081-24-2
+
286-08-8
双环[4.1.0]庚烷
+
1121-40-0
+
1121-41-1
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 0.5 h; Irradiation; Yield given;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 885 - 886
823-69-8
7,7-二氯二环[4.1.0]庚烷
→
反应条件
17081-24-2
+
286-08-8
双环[4.1.0]庚烷
+
18688-22-7
+
18688-21-6
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 8 h; Irradiationwithout LiAlH4.; Product distribution;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 885 - 886
108-90-7
氯苯
→
反应条件
17081-24-2
+
71-43-2
苯
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 0.5 h; Irradiationwithout LiAlH4.; Product distribution;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 885 - 886
