(4-甲氧基苄基)膦酸二甲酯合成路线 (共 5 条)
参考文献
Crenshaw, Michael D.; Zimmer, Hans
Journal of Organic Chemistry, 1983 , vol. 48, # 16 p. 2782 - 2784
参考文献
Griffin,C.E.; Gordon,M.
Journal of the American Chemical Society, 1967 , vol. 89, # 17 p. 4427 - 4431
反应条件
RefluxInert atmosphere;
参考文献
Lefebvre, Quentin; Jentsch, Marc; Rueping, Magnus
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1883 - 1890
反应条件
2: 1.) tert-butyllithium / 1.) THF/pentane, -78 deg C, 30 min; 2.) THF, reflux View Scheme
参考文献
Crenshaw, Michael D.; Zimmer, Hans
Journal of Organic Chemistry, 1983 , vol. 48, # 16 p. 2782 - 2784
反应条件
1: With potassium hydroxide; 18-crown-6 ether in dichloromethane T=20°C; Horner-Wadsworth-Emmons reaction; 2: With iodine in n-heptane Heating;
参考文献
Lee, Sang Kook; Park, Eun-Jung; Lee, Eunjung; Min, Hye-Young; Kim, Eun-Young; Lee, Taeho; Kim, Sanghee
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 9 p. 2105 - 2108