(8CI)-2-(p-甲氧基苯基)-呋喃合成路线 （共 51 条）
反应条件
Shvo's catalyst in acetone
T=65°C; 29 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Geissler, Diana
European Journal of Organic Chemistry, 2011 , # 25 p. 4814 - 4822
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex in toluene
T=50°C; 24 h;
参考文献
Denmark, Scott E.; Baird, John D.
Organic Letters, 2006 , vol. 8, # 4 p. 793 - 795
反应条件
1.1: 74 percent / dppp; Et3N / Pd(OAc)2 / acetonitrile / 16 h / Heating
2.1: Pcy3Cl2Ru=CHPh(diMesIm) / CH2Cl2 / 2 h / Heating
2.2: 79 percent / TFA / CH2Cl2 / 0.08 h / 20 °C
View Scheme
参考文献
Donohoe, Timothy J.; Orr, Allan J.; Gosby, Katherine; Bingham, Matilda
European Journal of Organic Chemistry, 2005 , # 10 p. 1969 - 1971
反应条件
C27H22Cl2N3NiP in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
12 h; Inert atmosphereSchlenk techniqueHeating;
参考文献
Zhang, Qiang; Zhang, Xue-Qi; Wang, Zhong-Xia
Dalton Transactions, 2012 , vol. 41, # 34 p. 10453 - 10464,12
反应条件
1: 87 percent / Grubbs' catalyst / CH2Cl2 / 0.5 h / 20 °C
2: 61 percent / MCPBA / CH2Cl2 / 20 °C
3: LiTMP / tetrahydrofuran / 20 °C
View Scheme
参考文献
Schmidt, Bernd; Wildemann, Holger
European Journal of Organic Chemistry, 2000 , # 18 p. 3145 - 3163
反应条件
iron (III) acetylacetonate in 1,3,4-trimethyl-imidazolidin-2-one
T=-25°C; 2.5 h;
参考文献
Haner, Jamie; Jack, Kelsey; Nagireddy, Jaipal; Raheem, Mohammed Abdul; Durham, Robin; Tam, William
Synthesis, 2011 , # 5 p. 731 - 738
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in PEG 300
T=55°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Silva, Aires da Conceicao; Senra, Jaqueline Dias; Aguiar, Lucia C.S.; Simas, Alessandro B.C.; Souza, Andrea Luzia F. de; Malta, Luiz Fernando Brum; Antunes
Tetrahedron Letters, 2010 , vol. 51, # 30 p. 3883 - 3885
反应条件
1: diethyl ether / 0 °C
2: DMP / CH2Cl2 / Ambient temperature
3: 4 percent / TCPCTFE / acetone
View Scheme
参考文献
Hashmi, A. Stephen K.; Ruppert, Thorsten L.; Knoefel, Thomas; Bats, Jan W.
Journal of Organic Chemistry, 1997 , vol. 62, # 21 p. 7295 - 7304
反应条件
1: 80 percent / (FSO2)2O, i-Pr2NEt / CH2Cl2 / 2 h / -78 °C
View Scheme
参考文献
Roth, Gregory P.; Fuller, Carl E.
Journal of Organic Chemistry, 1991 , vol. 56, # 11 p. 3493 - 3496
反应条件
1: N,N-dimethyl-formamide / 20 °C / |Inert atmosphere; |Schlenk technique
2: C27H22Cl2N3NiP / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 12 h / |Inert atmosphere; |Schlenk technique; |Heating
View Scheme
参考文献
Zhang, Qiang; Zhang, Xue-Qi; Wang, Zhong-Xia
Dalton Transactions, 2012 , vol. 41, # 34 p. 10453 - 10464,12
