in tetrahydrofuran (under inert atm., Schlenk); C6H4OCH3Sn(CH3)3 added to slurry of BiCl3 in THF, refluxed for 2 h; solvent removed in vacuo, CH2Cl2 added, filtered; monitored by NMR;
in tetrahydrofuran (under inert atm., Schlenk); C6H4OCH3Sn(CH3)3 added to slurry of BiCl3 in THF, refluxed for 2 h; solvent removed in vacuo, CH2Cl2 added, filtered; monitored by NMR;
参考文献
Mehring, Michael; Nolde, Christof; Schuermann, Markus
Inorganica Chimica Acta, 2009 , vol. 362, # 3 p. 745 - 752
