4-(N,N-二甲氨基)苯硼酸频那醇酯合成路线 （共 23 条）
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in dimethyl sulfoxide T=150°C; 0.333333 h; microwave irradiation;
参考文献
Appukkuttan, Prasad; Van Der Eycken, Erik; Dehaen, Wim
Synlett, 2003 , # 8 p. 1204 - 1206
反应条件
in dichloromethane 15 h;
参考文献
Andersen, Valdemar L.; Herth, Matthias M.; Lehel, Szabolcs; Knudsen, Gitte M.; Kristensen, Jesper L.
Tetrahedron Letters, 2013 , vol. 54, # 3 p. 213 - 216
反应条件
in tetrahydrofuran T=20°C;
参考文献
Chemical Communications, , # 35 p. 3667 - 3669
反应条件
palladium diacetate; triethylamine; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran; 1,4-dioxane T=100°C; 3 h;
参考文献
Broutin, Pierre-Emmanuel; Cerna, Igor; Campaniello, Maria; Leroux, Frederic; Colobert, Francoise
Organic Letters, 2004 , vol. 6, # 24 p. 4419 - 4422
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in 1,4-dioxane 17 h; Heating;
参考文献
Okamoto, Akimitsu; Tainaka, Kazuki; Nishiza, Ken-Ichiro; Saito, Isao
Journal of the American Chemical Society, 2005 , vol. 127, # 38 p. 13128 - 13129
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in dimethyl sulfoxide 6 h;
参考文献
Ishiyama, Tatsuo; Ishida, Kousaku; Miyaura, Norio
Tetrahedron, 2001 , vol. 57, # 49 p. 9813 - 9816
反应条件
copper(l) iodide; tributylphosphine; potassium tert-butylate in tetrahydrofuran byproducts: KBr, Me2NC6H5; react. of (B(OC(CH3)2)2)2 (1.5 equiv.), 4-Me2NC6H4Br (1 equiv.), CuI (10molpercent), nBu3P (13 molpercent) and KOtBu (1.5 equiv.) at room temp.;
参考文献
Kleeberg, Christian; Dang, Li; Lin, Zhenyang; Marder, Todd B.
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 5350 - 5354
Angewandte Chemie, 2009 , vol. 121, p. 5454 - 5458
反应条件
potassium acetate; bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in 1,4-dioxane T=80°C; 6 h;
参考文献
Ishiyama, Tatsuo; Ishida, Kousaku; Miyaura, Norio
Tetrahedron, 2001 , vol. 57, # 49 p. 9813 - 9816
反应条件
3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide in acetonitrile Zn dust (1.5 equiv., acid-activated) , CoBr2 (0.1 equiv.), stirred for 5min with allyl chloride (0.3 equiv.), a soln. of aryl halide (1 equiv.) and a soln. 1 equiv. of B compd. added at room temp., stirred for 30 mi n, tranesterificated with pinacol; hydrolized (NH4Cl), extd. (diethyl ether);
参考文献
Claudel, Stephanie; Gosmini, Corinne; Paris, Jean Marc; Perichon, Jacques
Chemical Communications, 2007 , # 35 p. 3667 - 3669
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=30°C; 0.166667 h; Inert atmosphere; 2: 4-bromo-N,N-dimethyl-aniline in ethylene glycol dimethyl ether T=30°C; 1 h;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
