4-甲氧基苯硼酸频那醇酯合成路线 (共 109 条)
反应条件
silica gel in water T=20°C; 0.5 h; Inert atmosphere;
参考文献
Molander, Gary A.; Cavalcanti, Livia N.; Canturk, Belgin; Pan, Po-Shen; Kennedy, Lauren E.
Journal of Organic Chemistry, 2009 , vol. 74, # 19 p. 7364 - 7369
反应条件
in tetrahydrofuran T=20°C;
参考文献
Chemical Communications, , # 35 p. 3667 - 3669
反应条件
3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide in acetonitrile Zn dust (1.5 equiv., acid-activated) , CoBr2 (0.1 equiv.), stirred for 5min with allyl chloride (0.3 equiv.), a soln. of aryl halide (1 equiv.) and a soln. 1 equiv. of B compd. added at room temp., stirred for 30 mi n, tranesterificated with pinacol; hydrolized (NH4Cl), extd. (diethyl ether);
参考文献
Claudel, Stephanie; Gosmini, Corinne; Paris, Jean Marc; Perichon, Jacques
Chemical Communications, 2007 , # 35 p. 3667 - 3669
反应条件
[2,2']bipyridinyl; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium T=80°C; 16 h; Title compound not separated from byproducts.;
参考文献
Journal of the American Chemical Society, , vol. 124, # 3 p. 390 - 391
反应条件
potassium acetate in tert-butyl alcohol T=90°C; 24 h; Inert atmosphere;
参考文献
Chow, Wing Kin; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 6913 - 6917
反应条件
Et3N; tetrabutylammonium iodide; 1,1'-bis-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane 100°C, 24 h; GC;
参考文献
Murata, Miki; Oda, Takeshi; Sogabe, Yosuke; Tone, Hirofumi; Namikoshi, Takeshi; Watanabe, Shinji
Chemistry Letters, 2011 , vol. 40, # 9 p. 962 - 963
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=30°C; 0.166667 h; Inert atmosphere; 2: 1-bromo-4-methoxy-benzene in ethylene glycol dimethyl ether T=30°C; 1 h; SolventTemperature;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; borylation; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 164 - 168
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; borylation; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 164 - 168
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; borylation; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 164 - 168