4-甲氧基苯硼酸频那醇酯合成路线 （共 109 条）
反应条件
methoxylamine hydrochloride; n-butyllithium in tetrahydrofuran; hexane T=-78 - 60°C; 24 h; Inert atmosphereCooling with acetone-dry ice; stereospecific reaction;
参考文献
Mlynarski, Scott N.; Karns, Alexander S.; Morken, James P.
Journal of the American Chemical Society, 2012 , vol. 134, # 40 p. 16449 - 16451,3
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium iodide in methanol; water T=80°C; 1 h; High pressure; Catalytic behavior; Reagent/catalystSolventTemperatureTime;
参考文献
Partridge, Benjamin M.; Hartwig, John F.
Organic Letters, 2013 , vol. 15, # 1 p. 140 - 143
反应条件
sodium hydroxide; hydroxylamine hydrochloride in ethanol T=20°C; 48 h;
参考文献
Kianmehr, Ebrahim; Yahyaee, Maryam; Tabatabai, Katayoun
Tetrahedron Letters, 2007 , vol. 48, # 15 p. 2713 - 2715
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium hydroxide in neat (no solvent) T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 18 p. 3553 - 3557
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium carbonate in tetrahydrofuran; water T=80°C; Suzuki-Miyaura cross-coupling;
参考文献
Kulhanek, Jiri; Bures, Filip; Ludwig, Miroslav
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. 11
反应条件
hydrogenchloride; polystyrene boronic acid in acetonitrile T=20°C; 18 h;
参考文献
Tetrahedron Letters, , vol. 45, # 35 p. 6657 - 6660
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide T=80°C; 18 h;
参考文献
Zhu, Lei; Duquette, Jason; Zhang, Mingbao
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3729 - 3732
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 8 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
反应条件
potassium phosphate; [NiCl(1-naph)(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 12 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
反应条件
potassium phosphate; [NiCl(1-naph)(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 4 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
