对甲氧羰基苯硼酸频哪醇酯合成路线 (共 33 条)
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in methanol T=20 - 40°C; Condensation; 8 h;
参考文献
Willis; Strongin
Tetrahedron Letters, 2000 , vol. 41, # 45 p. 8683 - 8686
反应条件
in acetone T=20°C; Inert atmosphere;
参考文献
Tsoi, Yuk-Tai; Zhou, Zhongyuan; Yu, Wing-Yiu
Organic Letters, 2011 , vol. 13, # 19 p. 5370 - 5373
反应条件
copper(l) iodide; tributylphosphine; potassium tert-butylate in tetrahydrofuran byproducts: KI; react. of (B(OC(CH3)2)2)2 (1.5 equiv.), 4-MeO2CC6H4I (1 equiv.), CuI (10molpercent), nBu3P (13 molpercent) and KOtBu (1.5 equiv.) at room temp.;
参考文献
Angewandte Chemie, International Edition, , vol. 48, p. 5350 - 5354
Angewandte Chemie, , vol. 121, p. 5454 - 5458
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; 2,2'-Bipyridine-4,4'-dicarboxylic acid in 2-methyl cyclohexane T=80°C; 12 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 50, # 45 p. 6176 - 6179
反应条件
potassium acetate in tert-butyl alcohol T=90°C; 2 h; Inert atmosphere;
参考文献
Chow, Wing Kin; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 6913 - 6917
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I) in octane 80°C, 16 h, methylbenzoate (5.0 mmol), bis(pinacolato)diboron (1.0 mmol), (Ir(OMe)(COD))2 (0.015 mmol);
参考文献
Chemical Communications, , vol. 46, # 1 p. 159 - 161
反应条件
1: p-aminobenzoic acid methyl ester With hydrogenchloride; sodium nitrite in water T=0 - 5°C; 2: With sodium tetrafluoroborate in water T=5°C; 3: 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane With copper(I) bromide in water; acetonitrile T=20°C; Sandmeyer type reaction; 4 h;
参考文献
Zhang, Jie; Wang, Xiaolong; Yu, Haitao; Ye, Jiahai
Synlett, 2012 , vol. 23, # 9 p. 1394 - 1396
反应条件
potassium phosphate; C4H11P2(1-)*2Cl(1-)*Ni(3+) in toluene T=100°C; 12 h;
参考文献
Organic Letters, , vol. 13, # 21 p. 5766 - 5769
反应条件
in diphenylether T=170°C; 15 h;
参考文献
Tetrahedron, , vol. 64, # 5 p. 866 - 873
Chemical Communications, , # 31 p. 3323 - 3325