(S)-(+)-扁桃酸合成路线 (共 229 条)
反应条件
1: dimethyl(phenyl)silyl chloride With lithium in tetrahydrofuran T=0°C; 12 h; Inert atmosphere; 2: benzaldehyde in tetrahydrofuran T=0°C; 0.333333 h; Inert atmosphere; 3: carbon dioxide With 1,3-dimethyl-imidazolidin-2-one T=60°C; P=760.051 Torr; 1 h;
参考文献
Organic Letters, , vol. 16, # 1 p. 14 - 17
反应条件
tetrabutylammonium halide in N,N-dimethyl-formamide Ambient temperatureelectrolysis, Mg anode;
参考文献
Mcharek, Slah; Heintz, Monique; Troupel, Michel; Perichon, Jacques
Bulletin de la Societe Chimique de France, 1989 , # 1 p. 95 - 97
反应条件
N,N-dimethyl-aniline in acetonitrile 2 h; Irradiation;
参考文献
Banerjee, Anamitro; Falvey, Daniel E.
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6245 - 6251
反应条件
fluorine in chloroform; water; acetonitrile T=0 - 20°C;
参考文献
Dayan, Sharon; Bareket, Yifat; Rozen, Shlomo
Tetrahedron, 1999 , vol. 55, # 12 p. 3657 - 3664
反应条件
samarium diiodide; water in tetrahydrofuran T=20°C; 0.2 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 53, # 8 p. 1017 - 1020
反应条件
pyridine; water; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol T=25°C; P=1748 Torr; 12 h; Mechanism;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3011 - 3018
反应条件
4-methyl-1,3-dioxolan-2-one; hydrogenchloride in water 6 h; Reflux;
参考文献
North, Michael; Omedes-Pujol, Marta
Beilstein Journal of Organic Chemistry, 2010 , vol. 6, p. 1043 - 1055
反应条件
sodium hydroxide T=120 - 125°C; 3 h;
参考文献
Bandyopadhyay; Bagchi; Podder; Moitra
Journal of the Indian Chemical Society, 1989 , vol. 66, # 4 p. 239 - 240
反应条件
methyl iodide; sodium tetrahydroborate in 1,4-dioxane; water T=20°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 11 p. 4151 - 4152
反应条件
calcium hydroxide powder; water; dichlorobis(trimethylphosphine)palladium in isopropyl alcohol T=100°C; 12 h; P(CO) = 150 atm at room temperature; further catalysts, solvents and hydroxide;
参考文献
Tetrahedron Letters, , vol. 28, # 24 p. 2721 - 2722