(S)-(+)-扁桃酸合成路线 (共 229 条)
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1119 - 1127
反应条件
2-hydroxyethanethiol in ethanol T=30°C; 5 h; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 103, # 8 p. 2070 - 2074
反应条件
pyridine; 3 A molecular sieve; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol T=25°C; P=1748 Torr; 12 h; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3011 - 3018
反应条件
sodium hydroxide; sodium hypochlorite; potassium chloride in methanol 3 h; Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 69, # 12 p. 1904 - 1908
反应条件
copper dichloride in methanol; water 3 h; Heating;
参考文献
Attanasi, Orazio; Filippone, Paolino; Serra-Zanetti, Franco
Synthetic Communications, 1982 , vol. 12, # 14 p. 1155 - 1162
反应条件
potassium carbonate Behandeln des Reaktionsprodukts mit wss. Natriumhydrogensulfit-Loesung und anschliessend mit Kaliumcyanid und Erhitzen des isolierten Reaktionsprodukts mit wss. Salzsaeure;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 2804,2805
反应条件
calcium hydroxide powder; dicobalt octacarbonyl; methyl iodide in 1,4-dioxane; water 20 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 52, # 12 p. 2623 - 2625
反应条件
calcium hydroxide powder; dicobalt octacarbonyl; methyl iodide in 1,4-dioxane; water 20 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 52, # 12 p. 2623 - 2625
反应条件
β-glucosidase T=30°C; 24 h;
参考文献
Phytochemistry (Elsevier), , vol. 24, # 10 p. 2438 - 2439
反应条件
1: 98 percent / Et3N; DMAP / CH2Cl2 2: 66 percent / DIPEA / CH2Cl2 3: 98 percent / TBAF / tetrahydrofuran 4: 92 percent / TEMPO; NAOCl; NaOCl2 / aq. phosphate buffer; acetonitrile / 55 °C / pH 6.5 5: 92 percent / ZnBr2 / CH2Cl2 View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 17 p. 3209 - 3213