反应条件
1: CH2Cl2 / 0.5 h / 0 °C 2: 1.) MeLi; 2.) tetrabutylammonium fluoride / 1.) THF, RT, 1 h; 2.) THF, 110 deg C, 10 h, sealed tube 3: 30 percent hydrogen peroxide 4: CH2Cl2 / 0.5 h / 0 °C 5: 1.) methyllithium / 1.) THF, 0 deg C, 1 h; 2.) THF, RT, overnight View Scheme
参考文献
Okazaki, Renji; Tokitoh, Norihiro
Journal of the Chemical Society, Chemical Communications, 1984 , # 3 p. 192 - 193
