3,5-二甲氧基苯甲酰氯合成路线 （共 90 条）
反应条件
1: diethyl ether 2: Ag2O 3: aqueous NaOH View Scheme
参考文献
Kondo et al.
Itsuu Kenkyusho Nempo, 1953 , # 4 p. 1,3; engl. Ref. S. 45, 48
Chem.Abstr., 1955 , p. 1075
反应条件
water; silver(l) oxide 1) Et2O; Yield given. Multistep reaction;
参考文献
Almeida, Wanda P.; Correia, Carlos Roque D.
Tetrahedron Letters, 1994 , vol. 35, # 9 p. 1367 - 1370
反应条件
3: fluoroboric acid, sodium nitrite / H2O View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
zinc(II) chloride T=25°C; 12 h;
参考文献
Asian Journal of Chemistry, , vol. 24, # 11 p. 5199 - 5201
参考文献
Journal of the American Chemical Society, , vol. 70, p. 662
反应条件
2,2'-azo-bisisobutyronitrile; trichloromonobromomethane; Fonderma 0.25 h; Heating;
参考文献
Dol, Georg C.; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
European Journal of Organic Chemistry, 1998 , # 2 p. 359 - 364
参考文献
Zeng, Dongli; Mi, Qixi; Sun, Hongfang; Wang, Haifang
Journal of Labelled Compounds and Radiopharmaceuticals, 2004 , vol. 47, # 3 p. 167 - 174
反应条件
1: (i) Mg(OEt)2, EtOH, Et2O, (ii) /BRN= 511839/ 2: aq. NH4Cl, aq. NH3 3: (i) NaOMe, Et2O, (ii) /BRN= 506456/, Et2O, (iii) aq. H2SO4 View Scheme
参考文献
Davies et al.
Journal of the Chemical Society, 1955 , p. 2782,2784
参考文献
Perez-Medrano, Arturo; Donnelly-Roberts, Diana L.; Honore, Prisca; Hsieh, Gin C.; Namovic, Marian T.; Peddi, Sridhar; Shuai, Qi; Wang, Ying; Faltynek, Connie R.; Jarvis, Michael F.; Carroll, William A.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 10 p. 3366 - 3376
反应条件
1: 70 percent / NaOAc, H2 / 10percent Pd-C / 2427.2 Torr / 1h, then 60 degC, overnight 2: 1.) Mg; MeI / diethyl ether / 1.) 3 h, reflux; 2.) 1 h, reflux 3: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
