in neat (no solvent) High Pressure; H2 pressure 150kg/cm**2, 200-235°C;;
参考文献
Koesster, R.; Bruno, G.; Binger, P.
Liebigs Annalen der Chemie, 1961 , vol. 644, p. 1 - 22
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Gmelin Handbook: B: B-Verb.14, 3.8.1.2.1, page 94 - 97
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反应条件
triethylamine byproducts: H2; TEA was added in 9 portions at -196°C, after each addition stirring 2 h at 0°C, 2 h at room temperature; then 4 days at room temperature; fractionated through traps, sepn. with fractionating volatiles;
参考文献
Journal of Organometallic Chemistry, , vol. 279, p. 359 - 372