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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
172217-04-8
合成路线
（共 13 条）
123-75-1
四氢吡咯
+
172217-04-8
→
反应条件
4030-18-6
1-乙酰基吡咯烷
反应条件
in tetrahydrofuran; ethanol; N,N-dimethyl-formamide T=-60°C; 48 h; Yield given;
参考文献
Murakami, Yasuoki; Kondo, Kazuhiro; Miki, Kazuki; Akiyama, Yoko; Watanabe, Toshiko; Yokoyama, Yuusaku
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3751 - 3754
172217-04-8
→
反应条件
4030-18-6
1-乙酰基吡咯烷
+
618-42-8
1-乙酰哌啶
反应条件
competition reaction with pyrrolidine and piperidine; EtOH-THF-DMF, 48 h, -60 deg C; Product distribution;
参考文献
Murakami, Yasuoki; Kondo, Kazuhiro; Miki, Kazuki; Akiyama, Yoko; Watanabe, Toshiko; Yokoyama, Yuusaku
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3751 - 3754
172217-04-8
+
100-46-9
苄胺
→
反应条件
588-46-5
N-苄基乙酰胺
反应条件
in ethanol 3 h; Ambient temperature;
参考文献
Murakami, Yasuoki; Kondo, Kazuhiro; Miki, Kazuki; Akiyama, Yoko; Watanabe, Toshiko; Yokoyama, Yuusaku
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3751 - 3754
172217-04-8
→
反应条件
588-46-5
N-苄基乙酰胺
+
36065-27-7
反应条件
competition reaction with benzylamine and α-methylbenzylamine; EtOH, 0 deg C, 2 h; var. solvent, temp., time; Product distribution;
参考文献
Murakami, Yasuoki; Kondo, Kazuhiro; Miki, Kazuki; Akiyama, Yoko; Watanabe, Toshiko; Yokoyama, Yuusaku
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3751 - 3754
172217-04-8
→
反应条件
588-46-5
N-苄基乙酰胺
+
29823-47-0
反应条件
competition reaction with benzylamine and N-methylbenzylamine; EtOH, 0 deg C, 2.5 h; Product distribution;
参考文献
Murakami, Yasuoki; Kondo, Kazuhiro; Miki, Kazuki; Akiyama, Yoko; Watanabe, Toshiko; Yokoyama, Yuusaku
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3751 - 3754
110-89-4
哌啶
+
172217-04-8
→
反应条件
618-42-8
1-乙酰哌啶
反应条件
in tetrahydrofuran; ethanol; N,N-dimethyl-formamide T=-60°C; 48 h; Yield given;
参考文献
Murakami, Yasuoki; Kondo, Kazuhiro; Miki, Kazuki; Akiyama, Yoko; Watanabe, Toshiko; Yokoyama, Yuusaku
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3751 - 3754
172217-04-8
→
反应条件
4030-18-6
1-乙酰基吡咯烷
+
618-42-8
1-乙酰哌啶
反应条件
competition reaction with pyrrolidine and piperidine; EtOH-THF-DMF, 48 h, -60 deg C; Product distribution;
参考文献
Murakami, Yasuoki; Kondo, Kazuhiro; Miki, Kazuki; Akiyama, Yoko; Watanabe, Toshiko; Yokoyama, Yuusaku
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3751 - 3754
74497-02-2
+
172217-04-8
→
反应条件
103-84-4
乙酰苯胺
反应条件
in ethanol 24 h; Heating;
参考文献
Murakami, Yasuoki; Kondo, Kazuhiro; Miki, Kazuki; Akiyama, Yoko; Watanabe, Toshiko; Yokoyama, Yuusaku
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3751 - 3754
172217-04-8
→
反应条件
23868-11-3
反应条件
1: 14 percent / K2CO3, Cu2Br2 / nitrobenzene / 25 h / 210 °C 2: 9.6 percent / KOH / 6 h / Heating View Scheme
参考文献
Murakami; Watanabe; Hagiwara; Akiyama; Ishii
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 8 p. 1281 - 1286
172217-04-8
+
585-32-0
Alpha,Alpha-二甲基苄胺
→
反应条件
79649-68-6
反应条件
in ethanol 24 h; Heating;
参考文献
Murakami, Yasuoki; Kondo, Kazuhiro; Miki, Kazuki; Akiyama, Yoko; Watanabe, Toshiko; Yokoyama, Yuusaku
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3751 - 3754
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