5-氯磺酰基-2-羟基苯甲酸合成路线 （共 17 条）
反应条件
chlorosulfonic acid T=70 - 80°C; 1.5 h;
参考文献
Obafemi, Craig. A.; Onigbinde, Adebayo O.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 57, # 1/2 p. 75 - 81
参考文献
Journal of the Chemical Society, , vol. 121, p. 2558
反应条件
chlorosulfonic acid 2 h; Ambient temperature;
参考文献
Cremlyn, Richard; Swinbourne, Frederick; Atherall, John; Courtney, Lynn; Cronje, Theo; at al.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 9, p. 155 - 164
反应条件
sulfuryl dichloride 0.166667 h; Ambient temperature;
参考文献
Lowe; Braden
Archiv der Pharmazie, 1995 , vol. 328, # 3 p. 283 - 285
参考文献
Zhurnal Obshchei Khimii, , vol. 20, p. 1818,1823; engl. Ausg. S. 1883, 1888
参考文献
Journal of the Chemical Society, , vol. 121, p. 2558
反应条件
hydrogenchloride; tin in water Cooling with iceReflux;
参考文献
Li, Jin-Ling; Gao, Zi-Wei; Sun, Ping; Gao, Ling-Xiang; Tikkanen, Wayne
Inorganica Chimica Acta, 2011 , vol. 368, # 1 p. 231 - 236
反应条件
1.1: iPr2NEt / dimethylformamide 2.1: dimethylformamide / 60 °C 2.2: polymer-supported HOBt; PyBrOP / dimethylformamide 2.3: isocyanate resin / tetrahydrofuran View Scheme
参考文献
Baxendale, Ian R.; Ley, Steven V.
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 17 p. 1983 - 1986
反应条件
1.1: iPr2NEt / dimethylformamide 2.1: dimethylformamide / 60 °C 2.2: polymer-supported HOBt; PyBrOP / dimethylformamide 2.3: isocyanate resin / tetrahydrofuran 3.1: 100 percent / NaOEt / ethanol / 0.17 h / 120 °C / microwave irradiation View Scheme
参考文献
Baxendale, Ian R.; Ley, Steven V.
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 17 p. 1983 - 1986
反应条件
sodium azide in water; acetone 5 h;
参考文献
Obafemi, Craig. A.; Onigbinde, Adebayo O.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 57, # 1/2 p. 75 - 81
