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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
172679-60-6
合成路线
（共 4 条）
110-89-4
哌啶
+
172679-60-6
→
反应条件
148868-55-7
反应条件
potassium carbonate in N,N-dimethyl-formamide 18 h; Ambient temperature;
参考文献
Yang, Donglai; Soulier, Jean-Louis; Sicsic, Sames; Mathe-Allainmat, Monique; Bremont, Beatrice; Croci, Tiziano; Cardamone, Rosanna; Aureggi, Giulio; Langlois, Michel
Journal of Medicinal Chemistry, 1997 , vol. 40, # 4 p. 608 - 621
172679-60-6
→
反应条件
307973-17-7
反应条件
1: 58 percent / acetonitrile / 18 h / 20 °C 2: 96 percent / anisole; CF3COOH / CH2Cl2 / 6 h View Scheme
参考文献
Curtet; Soulier; Zahradnik; Giner; Berque-Bestel; Mialet; Lezoualc'h; Donzeau-Gouge; Sicsic; Fischmeister; Langlois
Journal of Medicinal Chemistry, 2000 , vol. 43, # 20 p. 3761 - 3769
4093-28-1
对乙酰氨基-邻甲氧基苯甲酸甲酯
→
反应条件
172679-60-6
反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1: sodium hydroxide / N,N-dimethyl-formamide<br />2: N-chloro-succinimide / N,N-dimethyl-formamide<br />3: sodium hydroxide / ethanol<br />4: 4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane<br /> <br />
参考文献
Deng, Xin; Zhao, Xinxin; Han, Jing; Wang, Jingjie; Huang, Wenlong; Qian, Hai; Ge, Liang Letters in Drug Design and Discovery, 2012 , vol. 9, # 5 p. 489 - 493
65-49-6
4-氨基水杨酸
→
反应条件
172679-60-6
反应条件
<b>Multi-step reaction with 6 steps<br /> </b>1: sulfuric acid / 2 h / 20 °C<br />2: acetic acid / 1 h<br />3: sodium hydroxide / N,N-dimethyl-formamide<br />4: N-chloro-succinimide / N,N-dimethyl-formamide<br />5: sodium hydroxide / ethanol<br />6: 4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane<br /> <br />
参考文献
Deng, Xin; Zhao, Xinxin; Han, Jing; Wang, Jingjie; Huang, Wenlong; Qian, Hai; Ge, Liang Letters in Drug Design and Discovery, 2012 , vol. 9, # 5 p. 489 - 493
