3,5-二乙氧基基苯甲酸甲酯合成路线 （共 48 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate; benzyl chloride T=90°C; 0.5 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 52, # 41 p. 5319 - 5322
反应条件
sulfuric acid in benzene 2 h; Heating;
参考文献
Helvetica Chimica Acta, , vol. 63, # 6 p. 1425 - 1433
反应条件
1: With sodium hydroxide 3 h; 2: T=20°C; 3 h;
参考文献
Journal of Medicinal Chemistry, , vol. 55, # 10 p. 4551 - 4567
反应条件
sulfuric acid in chloroform
参考文献
, vol. No. 12, p. 2189 - 2215
反应条件
potassium carbonate in acetone T=55°C; 3 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 8 p. 1793 - 1798
反应条件
zinc(II) chloride T=25°C; 12 h;
参考文献
Asian Journal of Chemistry, , vol. 24, # 11 p. 5199 - 5201
参考文献
Justus Liebigs Annalen der Chemie, , vol. 296, p. 357
反应条件
potassium cyanide; water T=80°C; 24 h;
参考文献
Bulletin of the Korean Chemical Society, , vol. 32, # 6 p. 2070 - 2072
反应条件
1: 93 percent / toluene / 2.5 h / Heating 2: 8.7 g / sodium hydroxide (20percent) / 60 °C 3: 88 percent / conc. sulphuric acid / 16 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 2: 93 percent / toluene / 2.5 h / Heating 3: 8.7 g / sodium hydroxide (20percent) / 60 °C 4: 88 percent / conc. sulphuric acid / 16 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
