2-环己烯-1-酮缩二甲醇合成路线 (共 7 条)
反应条件
sodium methylate in methanol Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 50, # 24 p. 4844 - 4847
反应条件
1: Br2 2: NaOMe, DMSO View Scheme
参考文献
Journal of Organic Chemistry, , vol. 30, # 7 p. 2109 - 2120
反应条件
NiCl2((PPh3)P)2; (2S,3S)-chiraphos T=22°C; 15 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gomez-Bengoa; Heron; Didiuk; Luchaco; Hoveyda
Journal of the American Chemical Society, 1998 , vol. 120, # 30 p. 7649 - 7650
反应条件
sodium methylate in methanol Heating; Yield given. Yields of byproduct given;
参考文献
Taskinen, Esko; Nummelin, Kari
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4844 - 4847
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran T=22°C;
参考文献
Gomez-Bengoa; Heron; Didiuk; Luchaco; Hoveyda
Journal of the American Chemical Society, 1998 , vol. 120, # 30 p. 7649 - 7650
反应条件
sodium methylate in methanol Heating; Yield given. Yields of byproduct given;
参考文献
Taskinen, Esko; Nummelin, Kari
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4844 - 4847
反应条件
ClSO2F (sulfuryl chloride fluoride); epoxysulfonyl fluoride
T=-78°C;
参考文献
Forsyth,D.A.; Osterman,V.M.; Demember,J.R.
Journal of the American Chemical Society, 1985 , vol. 107, p. 818