1: With triethylamine; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide T=50°C; P=30003 Torr; 22 h; 2: With hydrogenchloride Further stages.;
1: 3-methyliodobenzene With magnesium in diethyl ether 0.5 h; Heating; 2: 1,8-diiodo-naphthalene With bis(acetylacetonate)nickel(II) in diethyl ether; benzene T=20°C;
参考文献
Journal of Organic Chemistry, , vol. 69, # 21 p. 7123 - 7133