2-甲基-2-丙基1-丁烯-3-炔-2-基氨基甲酸酯合成路线 （共 7 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78 - 20°C; Elimination;
参考文献
Saito, Shinichi; Uchiyama, Naoyuki; Gevorgyan, Vladimir; Yamamoto, Yoshinori
Journal of Organic Chemistry, 2000 , vol. 65, # 14 p. 4338 - 4341
反应条件
n-butyllithium in tetrahydrofuran 1) -78 deg C, 30 min; 2) -15 deg C, 15 min;
参考文献
Reginato, Gianna; Mordini, Alessandro; Caracciolo, Massimo
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6187 - 6192
反应条件
n-butyllithium in tetrahydrofuran 1) -78 deg C, 30 min; 2) -15 deg C, 15 min;
参考文献
Reginato, Gianna; Mordini, Alessandro; Caracciolo, Massimo
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6187 - 6192
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Branquet, Eric; Meffre, Patrick; Durand, Philippe; Le Goffic, Francois
Synthetic Communications, 1998 , vol. 28, # 4 p. 613 - 622
反应条件
n-butyllithium in tetrahydrofuran
参考文献
Branquet, Eric; Meffre, Patrick; Durand, Philippe; Le Goffic, Francois
Synthetic Communications, 1998 , vol. 28, # 4 p. 613 - 622
反应条件
1: 1.) PPh3, 2.) Et3N / 1) CH2Cl2, -20 deg C, 30 min; 2) CH2Cl2, -60 deg C, 30 min, rt, overnight 2: 5 percent / BuLi / tetrahydrofuran / 1) -78 deg C, 30 min; 2) -15 deg C, 15 min View Scheme
参考文献
Reginato, Gianna; Mordini, Alessandro; Caracciolo, Massimo
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6187 - 6192
反应条件
1: 1.) PPh3, 2.) Et3N / 1) CH2Cl2, -20 deg C, 30 min; 2) CH2Cl2, -60 deg C, 30 min, rt, overnight 2: BuLi / tetrahydrofuran / 1) -78 deg C, 30 min; 2) -15 deg C, 15 min View Scheme
参考文献
Reginato, Gianna; Mordini, Alessandro; Caracciolo, Massimo
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6187 - 6192
