9-(四氢-2-呋喃)腺膘呤合成路线 (共 6 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol P=2585.7 Torr; 15 h;
参考文献
Phadtare, Shashikant; Zemlicka, Jiri
Journal of the American Chemical Society, 1989 , vol. 111, # 15 p. 5925 - 5931
反应条件
1: 68 percent / aq. HCl / 18 h / Heating 2: 17 percent / aq. NaOH / dioxane / 1 h / Heating 3: 90 percent / H2 / 10percent Pd/C / ethanol / 15 h / 2585.7 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5925 - 5931
反应条件
1: 17 percent / aq. NaOH / dioxane / 1 h / Heating 2: 90 percent / H2 / 10percent Pd/C / ethanol / 15 h / 2585.7 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5925 - 5931
反应条件
1: 53 percent / K2CO3 / dimethylsulfoxide / 18 h / Ambient temperature 2: 68 percent / aq. HCl / 18 h / Heating 3: 17 percent / aq. NaOH / dioxane / 1 h / Heating 4: 90 percent / H2 / 10percent Pd/C / ethanol / 15 h / 2585.7 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5925 - 5931
反应条件
ethanesulfuric acid in ethyl acetate T=50°C;
参考文献
Thompson, Robert D.; Secunda, Sherrie; Daly, John W.; Olsson, Ray A.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 9 p. 2877 - 2882
反应条件
ammonium sulfate; caesium chloride; 1,1,1,3,3,3-hexamethyl-disilazane 2.) MeCN, 25 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Heterocycles, , vol. 31, # 2 p. 211 - 214