17356-08-0合成路线 （共 1741 条）
反应条件
sodium hydroxide; N-hexadecyl-N,N,N-trimethylammonium bromide in water; ethylenediamine High Pressure; cetyltrimethylammonium bromide dissolved (H2O, ethylenediamine); Cu(CH3COO)2 and CS(NH2)2 added to soln.; pH=12 of soln. adjusted by NaOH; sealed into autoclaves; Cu foil immersed in soln.; heated at 160°C for10 h; cooled to room temp.; XRD; TEM;
参考文献
Lv, Sa; Suo, Hui; Zhao, Xu; Wang, Chunxu; Zhou, Tieli; Jing, Shengyu; Xu, Yanan; Zhao, Chun
Journal of Alloys and Compounds, 2009 , vol. 479, # 1-2 p. L43-L46
反应条件
poly(vinylpyrrolidone) in N,N-dimethyl-formamide High Pressure; Cu salt dissolved in DMF, (H2N)2CS and poly(vinylpyrrolidone) added under stirring, treated in autoclave at 110-160°C for 15-30 h; cooled to room temp., ppt. centrifuged, washed (abs. EtOH), dried at 60-80°C for 6 h; elem. anal.; detd. by EDS, SEM;
参考文献
Liu, Jun; Xue, Dongfeng
Materials Research Bulletin, 2010 , vol. 45, # 3 p. 309 - 313
反应条件
ammonium hydroxide in water
参考文献
Maskaeva; Markov; Ivanov
Inorganic Materials, 2002 , vol. 38, # 9 p. 870 - 872
反应条件
in water High Pressure; stoich. amt. of salts were dissolved in the solvent, thioglycolic acid was added dropwise under stirring, 2 equiv. of thiourea was added, stirring for 30 min, teflon-lined autoclave, 160 °C for 20 h; cooling to room temp., ppt. was filtered off, washed with H2O and abs. EtOH several times, dried in vac. at 60 °C for 4 h;
参考文献
Gou, Xinglong; Peng, Shengjie; Zhang, Li; Shi, Yunhui; Chen, Jun; Shen, Panwen
Chemistry Letters, 2006 , vol. 35, # 9 p. 1050 - 1051
反应条件
sodium hydroxide; Ni(PEt3)2Cl2; sodium cyanoborohydride 1.) DMF, 60 deg C, 3 h, 2.) water, room temperature; Yield given. Multistep reaction;
参考文献
Takagi, Kentaro
Chemistry Letters, 1985 , p. 1307 - 1308
反应条件
ammonium sulfate 1.5 h; Heating;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 10 p. 2096 - 2099
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2380 - 2383
反应条件
ammonium sulfate T=170 - 175°C; 7 h; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 10 p. 2096 - 2099
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2380 - 2383
反应条件
dihydrogen hexachloroplatinate in tetrahydrofuran; isopropyl alcohol T=150°C; 21 h; Heatingampule; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 3 p. 621 - 624,550 - 552
参考文献
American Chemical Journal, , vol. 25, p. 177
参考文献
Shawali,A.S.; Abdelhamid,A.O.
Journal of Heterocyclic Chemistry, 1976 , vol. 13, p. 45 - 49
