boron trifluoride diethyl etherate T=40 - 46°C; 5 h; Inert atmosphere; Reagent/catalyst;

phosphoric acid; 5 palladium on charcoal; hydrogen T=80 - 105°C; P=7500.75 - 11251.1 Torr; 36 h; Inert atmosphereAutoclaveLarge scale;