1-苯基-3-丁炔-1-醇合成路线 （共 77 条）
反应条件
hydrogenchloride in tetrahydrofuran
T=25°C; 24 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
McCluskey; Muderawan; Muntari; Young
Journal of Organic Chemistry, 2001 , vol. 66, # 23 p. 7811 - 7817
反应条件
titanium(IV) isopropylate; iso-propylmagnesium bromide
1.) Et2O, -50 deg C to -40 deg C, 1 h; 2.) Et2O, -20 deg C, 0.5 h; Yield given. Multistep reaction;
参考文献
Nakagawa, Takashi; Kasatkin, Aleksandr; Sato, Fumie
Tetrahedron Letters, 1995 , vol. 36, # 18 p. 3207 - 3210
反应条件
n-butyllithium
1.) toluene, -78 deg C, 2.) toluene, -78 deg C; Yield given. Multistep reaction;
参考文献
Shinokubo, Hiroshi; Miki, Hiroaki; Yokoo, Toshiaki; Oshima, Koichiro; Utimoto, Kiitiro
Tetrahedron, 1995 , vol. 51, # 43 p. 11681 - 11692
反应条件
in tetrahydrofuran
T=0°C; other aldehydes and acyltrialkylsilanes, var. propargyl and allyl Grignard and zinc reagents; regioselectivity of alkylation; Product distribution;
参考文献
Yanagisawa, Akira; Habaue, Shigeki; Yamamoto, Hisashi
Journal of Organic Chemistry, 1989 , vol. 54, # 22 p. 5198 - 5200
反应条件
in tetrahydrofuran
0 deg C to r.t., 17 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
反应条件
indium in methanol; water
12 h; Ambient temperatureother reagent; Product distribution;
参考文献
Yi, Xiang-Hui; Meng, Yue; Hua, Xiao-Gang; Li, Chao-Jun
Journal of Organic Chemistry, 1998 , vol. 63, # 21 p. 7472 - 7480
反应条件
Yield given. Multistep reaction;
参考文献
McCluskey, Adam; Muderawari, I. Wayan; Muntari; Young, David J.
Synlett, 1998 , # 8 p. 909 - 911
反应条件
Yield given. Multistep reaction;
参考文献
McCluskey, Adam; Muderawari, I. Wayan; Muntari; Young, David J.
Synlett, 1998 , # 8 p. 909 - 911
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa; Habaue; Yamamoto
Tetrahedron, 1992 , vol. 48, # 11 p. 1969 - 1980
反应条件
ammonium chloride; zinc in water
1 h; various propargyl halides, acidic salt solutions or basic medium; various rate of products; Product distribution;
参考文献
Bieber, Lothar W.; Da Silva, Margarete F.; Da Costa, Rosenildo C.; Silva, Lilia O.S.
Tetrahedron Letters, 1998 , vol. 39, # 22 p. 3655 - 3658
