17beta-雌二醇 17-乙酸酯合成路线 （共 37 条）
参考文献
Gonzalez, A. G.; Jorge, Z. D.; Lopez Dorta, H.; Luis, F. Rodriguez
Tetrahedron Letters, 1981 , vol. 22, p. 335 - 336
反应条件
AlCl3, aluminium chloride; thiourea in dichloromethane T=20 - 30°C; 4.67 h; Heating / reflux;
参考文献
RICHTER GEDEON VEGYESZETI GYAR RT.
Patent: WO2006/61666 A2, 2006 ;
Location in patent: Page/Page column 14 ;
反应条件
C12F18O13Zn4 40 h; RefluxInert atmosphere; chemoselective reaction;
参考文献
Iwasaki, Takanori; Maegawa, Yusuke; Hayashi, Yukiko; Ohshima, Takashi; Mashima, Kazushi
Synlett, 2009 , # 10 p. 1659 - 1663
反应条件
copper(ll) bromide in acetonitrile 16 h; Ambient temperaturefurther addition of LiBr, var. amount of reagents, time, other 19-nor-Δ4-3-oxosteroids; Product distribution;
参考文献
Rao, Pemmaraju N.; Cessac, James W.; Kim, Hyun K.
Steroids, 1994 , vol. 59, # 11 p. 621 - 627
反应条件
boron trifluoride diethyl etherate in tetrahydrofuran T=0°C; 4.5 h;
参考文献
Nagao; Fujita; Kohno; Yagi
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 11 p. 3202 - 3207
反应条件
palladium; acetic acid Hydrogenolyse;
反应条件
1: pyridine / Ambient temperature 2: H2 / Pd/C / acetic acid / 3 h View Scheme
参考文献
Steroids, , vol. 45, # 3,4 p. 303 - 316
反应条件
1: H2, HCl / PtO2 2: aq. NaOH / ethanol 3: aq. HI View Scheme
参考文献
Steroids, , vol. 6, # 6 p. 841 - 844
反应条件
palladium on activated charcoal; ethyl acetate Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 72, p. 4534,4539
反应条件
copper diacetate 4 h; Heating;
参考文献
Horiuchi; Haga; Satoh
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 8 p. 2459 - 2462
