四乙基2,2'-联吡啶-4,4'-二基二(膦酸酯)合成路线 (共 2 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine; triphenylphosphine in toluene T=110°C; 6 h;
参考文献
Penicaud, Virginie; Odobel, Fabrice; Bujoli, Bruno
Tetrahedron Letters, 1998 , vol. 39, # 22 p. 3689 - 3692
反应条件
1: phosphorus oxytribromide / N,N-dimethyl-formamide / 19 h / 0 - 105 °C 2: tetrakis(triphenylphosphine) palladium(0); triethylamine / toluene / 4 h / 110 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Norris, Michael R.; Concepcion, Javier J.; Glasson, Christopher R. K.; Fang, Zhen; Lapides, Alexander M.; Ashford, Dennis L.; Templeton, Joseph L.; Meyer, Thomas J.
Inorganic Chemistry, 2013 , vol. 52, # 21 p. 12492 - 12501