2-(呋喃-2-基亚甲基)丙二酸二乙酯合成路线 （共 16 条）
反应条件
1: alcoholic potash 2: water; sodium amalgam 3: beim Destillieren View Scheme
参考文献
Marckwald
Chemische Berichte, 1888 , vol. 21, p. 1081
反应条件
1: 88 percent / hydrogen / Raney Ni / ethanol / 6 h / 80 °C / 56254.5 Torr 2: 76 percent / sodium ethoxide / ethanol 3: 60 percent / 85percent KOH / H2O; ethanol / 3 h / Heating View Scheme
参考文献
Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Miller, Vladimir; Vlkova, Marie; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 10 p. 2534 - 2544
反应条件
piperidine; acetic acid in toluene
1.) 100-104 deg C, 1.5 h, 2.) 110-120 deg C, 4 h.;
参考文献
Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Miller, Vladimir; Vlkova, Marie; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 10 p. 2534 - 2544
反应条件
zinc(II) iodide in tetrahydrofuran
P=7500600 Torr; 48 h;
参考文献
Sera, Akira; Ohara, Meguru; Kubo, Toshiaki; Itoh, Kuniaki; Yamada, Hiroaki; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 23 p. 5460 - 5464
反应条件
tri-n-butyl-arsine
T=80°C; 11 h;
参考文献
Shen, Yanchang; Yang, Baozhen
Journal of Organometallic Chemistry, 1989 , vol. 375, p. 45 - 50
反应条件
1: 87 percent / SiCl4 / CH2Cl2 / Ambient temperature
2: 68 percent / copper acetylacetonate / benzene / 48 h / Heating
3: 96 percent / CH2Cl2 / Irradiation
View Scheme
参考文献
Fujii, Takayoshi; Takahashi, Ohgi; Furukawa, Naomichi
Journal of Organic Chemistry, 1996 , vol. 61, # 18 p. 6233 - 6239
反应条件
1: hydrotalcite-2H / N,N-dimethyl-formamide / 3 h / 99.84 °C / |Inert atmosphere; |Schlenk technique
2: hydrotalcite-2H / N,N-dimethyl-formamide / 18 h / 99.84 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Shirotori, Mahiro; Nishimura, Shun; Ebitani, Kohki
Catalysis Science and Technology, 2014 , vol. 4, # 4 p. 971 - 978
参考文献
Knoevenagel
Chemische Berichte, 1898 , vol. 31, p. 2619
Chem. Zentralbl., 1898 , vol. 69, # II p. 695
参考文献
Marckwald
Chemische Berichte, 1888 , vol. 21, p. 1081
反应条件
hydrogen; nickel in ethanol
T=80°C; P=56254.5 Torr; 6 h;
参考文献
Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Miller, Vladimir; Vlkova, Marie; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 10 p. 2534 - 2544
