1-苯基乙醇-2,2,2-d3合成路线 （共 9 条）
反应条件
lithium aluminium tetrahydride in diethyl ether Ambient temperature;
参考文献
Hosokawa, Takahiro; Ohta, Toshiyuki; Kanayama, Satoshi; Murahashi, Shun-Ichi
Journal of Organic Chemistry, 1987 , vol. 52, # 9 p. 1758 - 1764
参考文献
Zimmermann, Gerhard; Ondruschka, Bernd; Nuechter, Matthias; Kopinke, Frank-Dieter; Remmler, Matthias
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 5 p. 415 - 420
反应条件
1: 70 percent / D2O, K2CO3, n-Bu4NHSO4 / benzene / 126 h 2: 99 percent / LiAlH4 / diethyl ether / Ambient temperature View Scheme
参考文献
Budzikiewicz, H.; Drabner, G.; Hammes, Ch.
Organic Mass Spectrometry, 1993 , vol. 28, # 11 p. 1326 - 1328
参考文献
Angelis; Smonou
Journal of Chemical Research - Part S, 2000 , # 10 p. 488 - 490
反应条件
in tetrahydrofuran 1 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Bapat, Jayant B.; Brown, Roger F.C.; Bulmer, Glenn H.; Childs, Trevor; Coulston, Karen J.; Eastwood, Frank W.; Taylor, Dennis K.
Australian Journal of Chemistry, 1997 , vol. 50, # 12 p. 1159 - 1182
反应条件
hydrogen bromide in benzene 1.5 h;
参考文献
Joly, Helen Alma; Westaway, Kenneth Charles
Canadian Journal of Chemistry, 1986 , vol. 64, p. 1206 - 1214
参考文献
Baumstark, Alfons L.; Vasquez, Pedro C.; Cunningham, Mark; Leggett-Robinson, Pamela M.
Heterocyclic Communications, 2010 , vol. 16, # 4-6 p. 217 - 220
参考文献
Balzer, Hartmut H.; Berger, Stefan
Magnetic Resonance in Chemistry, 1990 , vol. 28, # 5 p. 437 - 442
反应条件
potassium hydrogensulfate
T=230°C; P=975.08 Torr;
参考文献
Zimmermann, Gerhard; Ondruschka, Bernd; Nuechter, Matthias; Kopinke, Frank-Dieter; Remmler, Matthias
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 5 p. 415 - 420
